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Status:

Ob: Method "No longer supported"

  E: Errata

Method Book Page Status
Accelerated storage tests by heating, general methods (MT 46.1) F 149 Ob

Accelerated storage tests by heating, general methods (MT 46.2)

F 151
Accelerated storage tests by heating, combined methods (MT 46.3) J 128
Acephate [338], method H 5
Acetamiprid [649], method L 4
Acetone, anhydrous (RE 34) E 286
Acetone, soluble material, hot solution (MT 5.1) F 21

Acetone, solution at room temperature (MT 5.2)

F 22

Acetone, insoluble material (MT 27)

F 88
Acid wash test (MT 79) F 210 Ob
Adhesion to treated seeds (MT 194) N 145
Acidiy or alkalinity of formulation (MT 191)
L 143
Alachlor [204], method, TC, EC, GR D 4
Alachlor [204], method, CS E 4 Ob
Aldicarb [215], method H 10
Aldrin [27], method B 1707 Ob
d-Allethrin [742], method L 16
d-trans-Allerthrin [203], method H 52
alpha-Cypermethrin [454], method, TC, WP, EC, SC, UL H 14
alpha-Cypermethrin [454], method, SC (oil enhanced), WG K 4
alpha-Cypermethrin [454], method, LN M 40
alpha HCH, in lindane G 106
Alumina, Brockmann activity grade III (MT 50) 
F 156 Ob
Ametryn [133], method, GC H 22
Amidate, method E 142
Amines, identification of (MT 152) F 357 Ob
Aminocarb [293] D Ob

2-Aminopyridine, preparation of complexes of nitro compounds (MT 134)

F 328 Ob
Amitraz [362], method G 5
Amitrole [90], method, potentiometric 1B 1720 Ob
Amitrole [90], method, argentometric 1B 1722 Ob
Amitrole [90], method, HPLC J 4
Amitrole + monuron [90   + 99] argentometric 1B 1725 Ob
Amitrole + simazin [90   + 22] argentometric, WP 1B 1725 Ob
Amitrole + NH4CNS HPLC J 9
Amitrole + diuron [90 + 100] HPLC J 9
Amitrole + terbuthylazine [90 + 234] HPLC J 9
Ammonia solutions (RE 1) E 245
Ammonia-ammonium chloride buffer solution-pH 10 (MT 107) F 261
Ammonium cerium (IV) nitrate (RE 148) E 383
Ammonium hexanitratocerate (IV) (RE 148) E 383

d/Ammonium hydrogen citrate (RE 91)

E 362
Ammonium iron (III) sulphate, indicator solution (RE 2) E 246
d/Ammonium iron (II) sulphate, standard solutions (RE 38)  E 297
diAmmonium peroxosulphate (RE 132) E 375
Ammonium thiocyanate, standard solution (RE 3) E 249
Ammonium trioxovanadate (V), solution (RE 31) E 283
Anilazine [294], method E 5
Aromatic solvent naphtha (RE 62) E 328
Arsenic, determination of (MT 99) F 251
Arsenic in sulphur, method E 205
Arsenic in zineb, method E 231
Arsenic in ziram, method E 237
Arsenic (III) oxide, standard solution (RE 4) E 250
Asulam [240], method H 26
Atrazine [91], method, GC H 37
Attrition resistance of granules (MT 178) H 302

Attrition resistance of dispersible granules (MT 178.2)

K 140
Azadirachtin [627], method M 4
Azimsulfuron [584], method L 23
Azinphos-methyl [37], method, HPLC E 12
Azinphos-methyl [37], method, IR 1C 1970 Ob
Azoxystrobin [571], method M 0

Method Book Page Status
Barium hydroxide, standard solutions (RE 5)  E 251
Bendiocarb [232], method  D 10
Benfluralin [285], method, GC  1B 1728 Ob
Benfluralin [285], method, UV  1B 1726 Ob
Benfuracarb [501], method  H 38
Benomyl [206], method  D 14
Bensulfuron-methyl [502], method  K 6
Bensultap [464], method  E 17
Bentazone [366], method  1C 1973
Benzoylprop-ethyl [229], method  1B 1732 Ob
Benzoylprop-ethyl, pure (PP 229.a)  1B 1930
Beta-cyfluthrin [482], method  H 43
BHC (see HCH) Ob
BHTO in fenbutatin oxide  D 810
Bifenox [413], method  G 11
Binapacryl [138], method  D 67
Bioallethrin [203], method  H 52
Bioallethrin [203], TC, LV  L 31
Bioallethrin + piperonyl butoxide [203 + 33]  H 55
S-Bioallethrin [750], method, TC, LV  L 38
S-Bioallethrin [750], method, EW  M 18
2,2'-Bipyridyl (RE 61)  E 326
2,2'-Bipyridyl in diquat  H 161
4,4'-Bipyridyl (RE 60)  E 325
4,4'-Bipyridyl in paraquat  H 216
Bis (ethylenediamine) copper (II) sulphate (RE 81)  E 359
Bitertanol [386], method  J 14
Borax (RE 33)  E 376
Boscalid [673], method  N 4
Brodifacoum [370], method  1C 1981
Bromadiolone [371], method  E

23

Bromacil [139], method  1C 1986 Ob
Bromocresol green, solutions (RE 55)  E 317
Bromophenol blue, solution (RE 6)  E 254
Bromophos [5], method  1B 1738 Ob
Bromothymol blue, solutions (RE 7)  E 254
Bromoxynil [87], method  1C 1989
Bromoxynil pure (PP 87)  1C 2326
Bromoxynil - octanoate, GC method 1, TC  1C 1998 Ob
Bromoxynil GC method 2, TC,EC 1C 2004 Ob
Bromoxynil pure (PP 87.oct) 1C 2330
Bromoxynil - heptanoate H 57
Buffer solutions
Phosphate buffer (MT 19)  F 69
Bulk density (MT 186)  K 151
Bupirimate, identity test (MT 164)  F 406
Bupirimate [261], method  1C 2007 Ob
Bupirimate, pure (PP 261)  1C 2340
Butachlor [354], method  D 17 Ob
Butylate [266], method  1B 1744 Ob
Butylmagnesium chloride (RE 139)  E 379

Method Book Page Status
Cadmium, standard solution (RE 131) E 374
Captan [40], method, GC 1C 2015
Captan [40], method, HPLC 1C 2013
Carbaryl [26], method M 19
Carbendazim [263], method, UV H 61
Carbendazim [263], method, HPLC H 62
Carbetamide [95], method E 28
Carbon disulphide (RE 153) E 384
Carbofuran [276], method D 20
Carbosulfan [417], method E 35
Cartap [387], method D 24 Ob/E
Cerium (IV) sulphate, standard solutions (RE 99) E 368
Cetylpyridinium bromide, solution (RE 11) E 258
Chinomethionat [172], method 1C 2019 Ob
Chloramben[141], method 1B 1747 Ob
Chlordimeform [277], method D 28 Ob
Chlorfenvinphos [88], method H 67
Chloridazon [111], method D 31
Chloridazon [111], method extension WG H 76
Chlorides, in phenoxyalkanoic acids (MT 68.1) F 195 Ob
Chlorides, test for (MT 117) F 282 Ob
Chlorides, total chlorides (MT 100) F 254 Ob
Chlormequat [143], titration method D 39 Ob
Chlormequat, ion chromatographic method H 77
Chlorobenzilate [119], method H 81
4-Chloro-m-cresol (RE 104) E 371
4-Chloro-o-cresol (RE 109)  E 372
6-Chloro-p-cresol (RE 68)  E 335
1-Chloro-2,3-epoxyethane (MT 77) F 207 Ob
Chloroform (RE 64) E 330
Chloroform solubles, hot solutions (MT 87.1) F 221 Ob
Chloroform solubles, cold solutions (MT 87.2) F 222 Ob
6-Chloro-2-methylphenoxyacetic acid (RE 65) E 332
Gamma-Chlorophosphamidon, method E 182
Chloropropylate [120], method H 85
Chlorothalonil [288], method, TC, WP, WG, SC K 13
Chlorothalonil + HCB [288 + 161], method, TC, WP, WG, SC K 13
6-Chloro-o-tolyloxyacetic acid (RE 65)  E 332
Chloroxuron [187], method 1B 1751 Ob
Chlorphoxim, [341], method D 24
Chlorpropham [43], method 1B 1757
Chlorpropham + propham [43 + 63] 1C 2025
Chlorpyrifos [221], method, TC, DP, WP, EC, GR 1C 2028
Chlorpyrifos [221], method extension, UL K 23
Chlorsulfuron [441], method, TC, WG H 89
Chlorsulfuron [441], method extension WP K 24
Chlorthal [328], method, GC 1C 2032 Ob
Chlorthal [328], method, IR 1C 2034 Ob
Clofentezine [418], method G 18
Clothianidin [738], method N 14
Conductivity, determination of (MT 32) F 103
Congo red, solution (RE 9) E 256
Copper [44], method E 42
Copper ethylenediamine sulphate (RE 81) E 350
Copper, water soluble F
Colorimetric method with bathocuproine (98.1) F 246
Atomic absorption method (MT 98.2) H 248
Copper + mancozeb [44 + 34], method H 96
Copper + maneb [44 + 61], method H 100
Copper + zineb [44 + 25], method H 100
Copper + ziram [44 + 31], method F 101
Correction of interfering peaks (MT 114) F 278 Ob
Coumatetralyl [189], method G 24
m-Cresol (RE 100) E 370
o-Cresol (RE 70) E 338
p-Cresol (RE 101) E 370
Crystal violet, solution (RE 129)  E 373
Cyanazine [230], method  1C 2039
Cyanazine, pure (PP 230) 1C 2335
Cycloate [214], method H 102
Cyclohexane (RE 155) E 386
Cycloxydim [510], method K 25
Cyfluthrin [385], method H 106
beta-Cyfluthrin [482], method H 43
Lambda-Cyhalothrin [463], method, TC, WP, EC, UL E 49
Lambda-Cyhalothrin [463], method, LN N 83
Lambda-Cyhalothrin [463], method, CS K 86
Lambda-Cyhalothrin, free, determination in CS formulations (MT 189) L 137
Lambda-Cyhalothrin, determination of release properties CS formulations (MT 190)  L 140 E
Cyhexatin [289], method D 46
Cymoxanil [419], method J 22
Cypermethrin, identity test (MT 163) F 404
Cypermethrin [332], method, GC 1C 2047 Ob
Cypermethrin [332], method, diastereomeric ratio, HPLC
1C 2052
Alpha-Cypermethrin [454], method, TC, WP, EC, SC, UL H 14
alpha-Cypermethrin [454], method, SC (oil enhanced), WG K 4
alpha-Cypermethrin [454], method, LN M 40
Cyphenothrin [805], method M 44
Cyproconazole [600], method J 29
Cyprodinil [511], method N 25
Cyromazin [420], method M 54

Method Book Page Status
2,4-D [1], method,  titration method  1C  2060
2,4-D [1], method,  GC, titration method  1C  2061
2,4-D [1], method, HPLC, titration method  1C  2062
2,4-D [1], method,  salts, titration method  1C  2063
2,4-D [1], method,  salts, titration method, GC  1C  2065
2,4-D [1], method,  salts, titration method, HPLC  1C  2065
2,4-D [1], method,  esters, titration method  1C  2068  Ob
2,4-D [1], method,  esters, titration method, GC  1C  2069
2,4-D [1], method,  esters, titration method, HPLC  1C  2071
2,4-D + dicamba [1+85] (salts), GC  1C  2071
2,4-D + dicamba [1+85] (salts), IR  H  133
2,4-D + dicamba + mecoprop [1 + 85 + 51] (salts)  D  51
2,4-D + picloram [1 + 174]  1B 1757  Ob
2,4-D + 2,4,5-T [1 + 6] (esters)  1C  2072
2,4-D, pure (PP 1)  1C  2307
Dalapon [52], method (Na + Mg salt)  D  54
Dazomet [146], method, CS2 method  1C  2074
Dazomet [146], method, CS2 method HPLC  J  37
2,4-DB [83], method  1C  2078
2,4-DB [83], K salt,  titration method  1C  2080
2,4-DB [83], GC  1C  2082
2,4-DB, pure (PP 83)  1C  2321
DDT [3], method   E  58
DDT [3], DDT + endrin [3 + 28]  1B  1760  Ob
Deltamethrin [333], method, TC, WP, EC, UL, DP  D  57
Deltamethrin [333], TC, WG, WP, EC, SC, DP, EG, EW, UL, WT (replaced)  L  45
Deltamethrin [333], TB, LN  M  65
Deltamethrin [333], LN  N  34
Desmetryn [147], method, GC  1B  1766  Ob
Desmetryn [147], method, titration method  1B  1765  Ob
Deniges reagent (RE 57)  E  319
Deschlorophosphamidon, method  E  182
Detection and identification of impurities in substituted phenylurea herbicides (MT 142)  F  336  Ob
Determination of organochlorine pesticides in aqueous emulsions (MT 65)  F  190  Ob
Determination of pH values, general method (MT 75.1)  F  205  Ob
pH of aqueous dispersions (MT 75.2)  F  206  Ob
pH of diluted and undiluted aqueous solutions (MT 75.3)  J  131  E
Determination of seed-to-seed uniformity of distribution for liquid seed-treament formulations (MT 175) F  438
Diazinon [15], method  H  122
Diazomethane (RE 35)  R  286
1,2-Dibromoethane [125], method  1C  2115  Ob
Dicamba [85], method, infrared method  H  127
Dicamba [85], method, HPLC method  K  32 E
Dicamba + 2,4-D [85 + 1], method  H  133
Dicamba + MCPA [85 + 2], method  H  131
Dicamba + 2,4-D + mecoprop [85 + 1 + 51] (salts)  D  51
Dichlobenil [73], method, GC(cap)  E  65
Dichlobenil [73], GC  1B  1769  Ob
Dichlofluanid [74], method, titration method  1B  1774  Ob
Dichlofluanid [74], method, HPLC  1C  2083
2,4-Dichlorobenzoic acid (RE 79)  E  347
Dichlorodifluoromethane insoluble material (MT 16)  F  52  Ob
2,4-dichloroanisole  G  14
4,6-Dichloro-2-methylphenoxyacetic acid (RE 66)  E  333
2,4-dichlorophenol  G  14
4,6-Dichloro-o-tolyloxyacetic acid (RE 66)  E  333
2,6-Dichlorophenol (RE 72)   E  339

4,6-Dichloro-o-cresol (RE 69) 

 E  335
Dichlorprop [84], method, titration method
 1C  2087
Dichlorprop [84], method, GC  1C  2087 Ob
Dichlorprop [84], method, HPLC  1C  2088
Dichlorprop [84], HPLC  G  32
Dichlorprop [84], method, salts, titration method  1C  2092
Dichlorprop [84], method, salts, GC  1C  2093
Dichlorprop [84], method, salts, HPLCDinitro compounds, solubility of salts and alkali insolubles (MT 108) 1C 2093 Ob
Dichlorprop, pure (PP 84) 1C 2323
dichlorprop-P [476], method G 32
Dichlorvos [11], method, GC H 135
Diclofop [358], method 1C 2096 Ob
Dicofol [123], method D 67
Dieldrin [16], method 1B 1781
Diethyl ether (RE 12) E 258
Diflovidazin [734], method L 61
Diflubenzuron [339], method, TC, WP H 141
Diflubenzuron [339], method, TC, WP (revised methods) N 38
Diflubenzuron [339], method, SC, GR, TB N 42
Diflufenican [462], method H 147
Diisopropyl ether (RE 63) E 328
Dilute emulsion stability (MT 20) F 71 Ob
Dilute emulsion stability, colorimetric method (MT 173) F 431
Dilution stability (MT 41) F 131  E
Dimedone derivative (MT 28) F 89 Ob
Dimercury dicyanide oxide (RE 154) E 383
Dimethoate [59], HPLC method E 69
Dimethoate [59], GLC method H 153
Dimethomorph [483], method G 39
O,O-Dimethyl S-methylcarbamoylmethylphosphorodithioate (RE 86) E 359
O,O-Dimethyl methylphosphoroamidothioate, method E 142
O,S-Dimethyl methylphosphoroamidothioate, method E 142
O,S-Dimethyl 4-nitrophenylphosphorothioate, method E 169
O,O-Dimethyl phosphoroamidothioate, method E 142
Dimethyl sulphate (RE 13) E 259
Dinotefuran [749], method L 67
Dinoterb [238], method 1B 1797 Ob
Dinitro compounds, solubility of salts and alkali insolubles (MT 108) F 262 Ob
Dinitro compounds, solubility of mineral acidity of (MT 109) F 263 Ob
Dioxane (RE 49) E 311
Diquat [55], method

E

74 Ob
Diquat [55], method, identity test G 47
Diquat [55], method free 2,2'-bipyridyl H 161
Diquat [55], method terpyrides in M 68
Diquat dibromide (PP 55) E 387  E
Dispersion stability of suspo-emulsions (MT 180)  H 310
Dissolution rate of water-soluble bags (MT 176) F 440
Disulfoton [152], method 1C

2101

Ob
dithianon [153], method, HPLC G 50
dithianon [153], method, colorimetric 1C 2105 Ob
Dithiocarbamates, determination of anions (MT 154) F 361
Identity test for certain alkylenebis (dithiocarbamates) (MT 130) F 320
Qualitative procedure for confirmation of the presence of a dithiocarbamate or thiuram disulphide (MT 153) F 360
Dithizone (RE 59) E 371
Dodine [101], method 1B 1802 Ob/E
Dustability test after accelerated storage (MT 34) F 107 Ob
Dust content and apparent density of granular formulations, sampling (MT 58.1) F 173 Ob/E
Dust content and apparent density of granular formulations, preparation of the sample (MT 58.2) F 173 Ob/E
Dust content and apparent density of granular formulations, apparent density after compactation without pressure (MT 58.3) F 175 Ob/E
Dustiness of granular products (MT 171) F 425

Method Book Page Status
Edifenphos [409], method  E  79
EDTA sodium salt, solutions (RE 37)  E  295
Emulsion characteristics of emulsifiable concentrates, five per cent v/v oil phase when diluted (MT 36.1)
 F  108 Ob
Emulsion characteristics of emulsifiable concentrates, dispersion stability of aqueous emulsions (MT 36.2)  F  112 Ob
Emulsion characteristics of emulsifiable concentrates, emulsion characteristics and re-emulsification properties (MT 36.3)  K 137
Emulsion characteristics of emulsifiable concentrates, dilute, colorimetric determination of the stability of emulsions (MT 173)  F 431
Emulsion characteristics of emulsifiable concentrates, dilute, agrochemical emulsion tester MT 183)  J 138 Ob
Endosulfan [89], method  IC 2111 Ob
Endrin [28], method
 1B 1805 Ob
Endrin + DDT [28 + 3]  1B

1760

Ob
Endrin + parathion-methyl [28 + 487]  1B 1819 Ob
Epichlorhydrin (MT 77)  F 207 Ob
Epoxiconazole [609], method
 K 38
EPTC [155], method  1B 1823 Ob
Erichrome Black T (RE 53)  E 316
Esbiothrin [751], method

 L

73
Esfenvalerate [481], method  K 47
Ethanol soluble material, hot solution (MT 7.1)  F 23
Ethanol soluble material, solution at room temperature (MT 7.2)  F 24
Ethephon [373], method  H  165
Ethiofencarb [363], method  E  84
Ethion [102], method  1B  1826
Ethirimol, identity test (MT 164)  F  406
Ethirimol [242], method  D  72 Ob
Ethofumesate [233], method  J  43
Ethofumesate [233], SE  L  80
Ethyl butylacetamidopropionate [667], method  M  76
N-(2-ethylhexyl)-8,9,10-tribornene-2,3-dicarboxamide [345], method  1C  2166
Ethylenediamine tetraacetic acid, sodium salt, solutions (RE 37) 
 E  295
Etofenprox [471], method (packed column)  G  56
Etofenprox [471], method (capillary column)  K  57
ETU, determination in ethylenebisdithiocarbamates (MT 162)  F  399  E
Evaluation of wettability, wetting time of a standard type (MT 53.1)  F  160
Evaluation of wettability, wetting of leaf surfaces (MT 53.2)
 F  162
Evaluation of wettability, wetting of dispersible powders (MT 53.3)  F  164
Extractable acids, determination of (MT 126)
 F  288
Extractable acids, melting point of (MT 127)  F  291

Method  Book Page
 Status
Fat extraction apparatus (MT 67) F  194 Ob
Fehling's solution (RE 29) E  262  
Fenbutatin oxide [359], method D 77  
Fenhexamid [603], method M 80  
Fenitrothion [35], method N 46  
Fenitrothion [35], method from CIPAC 1C p 2117 was replaced      
Fenobucarb [390], method, TLC D 87 Ob
Fenobucarb [390], method, HPLC D 89 Ob
Fenoprop [118], method, titration method 1C 2121  
Fenoprop [118], method, GC 1C 2122 Ob

Fenoprop [118], method, salts, titration method 

1C 2122  
Fenoprop [118], method,GC 1C 2123  
Fenoprop, pure (PP 118) 1C 2333  
Fenoxaprop-P [484], method, TC, EW J 51 Ob
Fenoxaprop-P [484], method, TC, EW, EC, SE, OD M 89  
Fenpropimorph [427], method G 62  
Fensulfothion [303], method, HPLC 1C 2126 Ob
Fensulfothion [303], method, GC D 92 Ob
Fenthion [79], method, col  1B 1830 Ob
Fenthion [79], method GC, TC, WP, GR, EC, EW L 81  
Fenthion [79], method UL, DP M 96  
Fentin acetate [489], method E 89  
Fentin acetate + maneb [489 + 61], GC 1B 1840 Ob
Fentin acetate + maneb [489 + 61], HPLC E 3  
Fentin hydroxide [490], method E 94  
Fentin hydroxide + maneb [490 + 61] GC 1B 1840 Ob
Fentin hydroxide + maneb [490 + 61] HPLC
E 93  
Fenvalerate, identity test (MT 163) F 404  
Fenvalerate [334], method, TC D 101  
Fenvalerate [334], method, EC G 68  
Ferroin sulphate, solution (RE 149) E 383  
Fipronil [581], method TC, EC, UL J 60  
Fipronil [581], method PS, SC, WG, GR, FG N 60  
Flash point, Abel method (MT 12.1) F 31  
Tag closed tester (MT 12.2) F 37  
Pensky-Martens closed tester (MT 12.3) F 40  
Flowability, of powders (MT 44) F 145  
Flowability, of water dispersible granules (MT 172) F 430 E
Fluazifop-butyl [395], method D 106  
Fluazifop-P-butyl [467], method G 71  
Flufenoxuron [470], method M 98  
Fluometuron [159], method 1B 1842 Ob
Flusilazole [435], method H 171  
Folpet [75], method 1B 1845  
Foaming, persistent (MT 47.1) F 152 Ob
Foaming, of suspension concentrates (MT 47.2) F 152  
Formaldehyde [156], method 1C 2130 Ob
Formothion [160], method H 178  
Fosetyl [384], method, titration method G

82

 
Fosetyl [384], method, HPLC J 66  
Free acidity or alkalinity, methyl red indicator method (MT 31.1) F 96  
Free acidity or alkalinity, electrometric prodedure (MT 31.2)
F 98  
Free acidity or alkalinity, acidity of petroleum products (MT 31.3) F 99  
Free acidity or alkalinity of formulations (MT 191) L 143  
Free acidity of phenoxyalkanoic esters (MT 66) F 193 Ob
Free amines in urea herbicides (MT 141) F 333 Ob
free 2,2’-bipyridyl in diquat H 161  
free 4,4’-bipyridyl in paraquat H 216  
Free lambda-cyhalothrin in CS formulations (MT 189) L 137  
Free parathion-methyl in CS formulations (MT 188) L 132  
Free phenols in phenoxyalkanoic herbicides, GLC method (MT 69) F 197  
Free phenols in phenoxyalkanoic herbicides, HPLC method (MT 155) F 362  
Freezing mixtures, ( 5 ± 1°C) (MT 14.1) F 44  
Freezing mixtures, (10 ± 1°C) (MT 14.2) F 44  
Freezing point (MT 1) F 3  
Friability of tablets (MT 193) L 147  

 


Method  Book Page
 Status
Gas chromatography of phenoxyalkanoic acids and other herbicides (MT 129)  F 292 Ob
Glufosinate [437], method G 89  
Glyphosate [284], method, TC, SL 1C 2132  
Glyphosate [284], method, SG  H 182  

 

Method  Book Page
Status
Icaridin [740], method K  64  
Identification of amines (MT 152) F 357 Ob
Identification of urea herbicides (MT 137)
F 329 Ob
Identity test for certain dithiocarbamates and thiram and their mixtures (MT 130) F 321  
Identity tests for permethrin, cypermethrin and fenvalerate (MT 163)  F 404  
Identity tests for pirimicarb, bupirimate, ethirimol, pirimiphos-ethyl and pirimiphos-methyl (MT 164)  F 406  
Ignition tests, assessment of spontaneous ignition potential of dithio-carbamates (MT 84.1)  F 218  
Imazalil [335], method E 95 Ob
Imidacloprid [582], method, TC, WP, SC, GR, fertilizer formulations H 185  
Imidacloprid [582], method, TC, WG, SC, WS, FS K 70  
Imidacloprid [582], method, SL, OD L 89  
Indoxacarb, [612], method N 73  
Iodides, test for (MT 118) F 283 Ob
Iodine, standard solutions (RE 16) E 264  
Iodine, monochloride, solution (RE 58)  E 320  
Ioxynil [86], method E 101  
Ioxynil octanoate [86.407], method G 94  
Iprobenfos [393], method D 110 Ob
Iprodione [278], method G 98  
Iprodione [278], WG L 90  
IR 3535 see Ethyl butylacetamidopropionate      
Iron, determination of (MT 95)  F 236  
Iron (III) chloride (RE 84) E 355  
Isobutyl benzoate (RE 92) E 362  
Isochloridazone D 35  
Isofenphos [412], method D 114  
Isolation of active ingredient, extraction with acetone (MT 37.1) F 115 Ob
Isolation of active ingredient, extraction with light petroleum (MT 37.2)
F 115 Ob
Isomalathion, method 1B 1855  
Isoprocarb [396], method D 118 Ob
Isoprothiolane [456], method E 105 Ob
Isoproturon [336], method E 110  

Method  Book Page
Status
Malathion [12], method, TC, DP, WP, EC, OL, (GLC, packed column)  1B 1849 Ob
Malathion [12], method, TC, EC, EW, DP, (GLC, capillary column)  K 88  
Mancozeb [34], method H 194  
Mancozeb [34], method + copper [34 + 44] H 96  
Manganese, bismuthate method (MT 93.1) F 232  
EDTA method (MT 93.2) E 234  
Magnesium sulphate, solution (RE 144) E 381  
Maneb [61], method E 116 E
Maneb+ copper [61+ 449] H 100  
Maneb+ fentin [61 + 103] E 89  
Maneb+ fentin acetate [61 + 489] D 95  
Maneb+ fentin hydroxide [61 + 490] D 98  
MCPA [2], titration method 1C 2137 Ob
MCPA [2], GC 1C 2138 Ob
MCPA [2], HPLC 1C 2139  
MCPA [2] - salts,  titration method 1C 2141 Ob
MCPA [2] - salts, GC 1C 2141  
MCPA [2] - salts, HPLC 1C 2141  
MCPA [2] - esters, titration method
1C 2145 Ob
MCPA [2] - esters, GC
1C 2145 Ob
MCPA [2] - esters, HPLC 1C 2145  
MCPA + 2,3,6-TBA [2 + 49] 1C 2148 Ob
MCPA, pure (PP 2) 1C 2309  
MCPB [50], titration method 1C 2153 Ob
MCPB [50], GC
1C 2154 Ob
MCPB [50] - salts, titraton method 1C 2154 Ob
MCPB [50] - salts, GC
1C 2155 Ob
MCPB, pure (PP 50) 1C 2316  
Mecoprop [51], titration method 1C 2157  
Mecoprop [51], GC 1C 2158 Ob
Mecoprop [51], HPLC 1C 2158  
Mecoprop [51] - salts,  titraton method
1C 2162  
Mecoprop [51] - salts,  GC
1C 2163 Ob
Mecoprop [51] - salts,  HPLC
1C 2163  
Mecoprop+ 2,4-D + dicamba [51 + 1 + 8](salts) D 51  
Mecoprop, pure (PP 51) 1C 2319  
Mecoprop-P [475], method  G 109  
Mefenpyr-diethyl, [651.229], method N 87  
Melting point (MT 2) F 5  
Mepiquat [440], method J 78  
Mercurial impurities in technical and formulated mercury compounds (MT 110) F 264  
Mercury, determination on treated seed (MT 158)  F 387 Ob
Mercuric oxycyanide (RE 154) E 385  
Mercury(II)chloride (RE 135) E 378  
Mercury(II) salts, characteristic reactions of (MT 116) F 280 Ob
Mercury(II)sulphate, solution (RE 57) E 319  
Metalaxyl [365], method E 123  
Metamitron [381], method D 124  
Metam-sodium [20], method E 131  
Metazachlor [411], method E 134  
Methabenzthiazuron [201], method  G 116  
Methamidophos [355], method E 139  
Methanol (RE 47) E 309  
Methiocarb [165], method D 130  
Methomyl [264], method H 199  
Methoprene [414], method M 115  
Methoprotryne [94], method 1B 1864 Ob
N-Methyl amidate, method E 142  
1-Methylcyclopropene [767], method  N 99  
Methyl (dimethoxyphosphinothioylthio) acetate (RE 88) E 360  
Methyl-methamidophos, method  E 142  
Methyl orange, solutions (RE 17) E 266  
2-Methylphenoxyacetic acid (RE 67) E 334  
Methyl red, solutions (RE 18) E 266  
Methyl undec-10-enoate (RE 89.2) E 361  
Metolachlor [400], method D 134  
Metribuzin [283], method D 137  
Metsulfuron [441], method, TC, WG H 204  
Metsulfuron [441], method extension WP K 95  
Mevinphos [45] H 212  
MGK 264 + pyrethrum + piperonylbutoxide [345 + 32 + 33 ], method H 239  
Mineral acidity of dinitrocompounds (MT 109) F 263 Ob
Miscibility with hydrocarbon oil (MT 23) F 85  
Neutrality (MT 74) F 204  
Mineral oil (RE 36) E 292  
Molinate [235], method  1B 1866 Ob
Monocrotophos [287], method E 145  
Mordant black, solutions (RE 53) E 316  

Method Book  Page  Status  
Packing of columns for gaschromatography (MT 149)  F 349
Ob
Palmitic acid (RE 80)  E 348  
Paraffin, liquid (RE 8) E 255  
Paraquat [56], aqueous solutions, method E 166 Ob
Paraquat [56], aqueous solutions, identity tests G 128  
Paraquat [56], aqueous solutions, free 4,4’-bipyridyl H 216  
Paraquat [56], aqueous solutions, terpyridines in M 141  
Paraquat + diquat [55 + 56], method  E 75 Ob
Paraquat dichloride (PP 55) E 390  
Parathion [10], method, GC  1B 1875 Ob
Parathion [10], method, HPLC 1B 1876 Ob
Parathion-methyl [487], method, GC, TC, WP, EC 1B 1879 Ob
Parathion-methyl [487], method, HPLC, TC, EC 1B 1881 Ob
Parathion-methyl [487], method, HPLC, CS 1C 2169 Ob
Parathion-methyl [487], method, GC, Ol, DP E 171 Ob
Parathion-methyl [487], method, HPLC, OL E 171 OB
Parathion-methyl, free, determination in CS formulations (MT188)  L 132  
Parathion-methyl, free, HPLC, determination of S-methyl isomer in TC E 169  
Parathion-methyl, free, HPLC, determination of S-methyl isomer in SC E 172  
Particle sizean alysis by laser diffraction (MT 187) K 153  
Particle size, formulations without carriers (MT 42.1)  F 133 Ob
Particle size, formulations formulations containing carriers (MT 42.2)
F 138 Ob
Particle size distribution of a DDT dispersible powder (MT 43)  F 140 Ob
PCAF Reagent (RE 146) E 382  
Pebulate [236], method  1B 1887 Ob
Pencycuron [402], method E 173  
Pendimethanil [357], method M 148  
Pentacyanoaminoferroate (RE 146) E 382  
Perchloric acid, standard solutions (RE 43) E 304  
Permethrin, identity test (MT 163) 

F

404  
Permethrin, method, TC, WP, EC, WG, DP IC 2173  
Permethrin, TC, EW, LN M 155  
Persistent foaming (MT 47.1)  F 152 Ob
Petroleum spirit (RE 45) E 307  
pH, determination of (MT 75)  F 205 Ob
pH, determination of revised method (MT 75.3)  J 131  
Phenmedipham [77], method, titration method 1C 2181  
Phenmedipham [77], method, HPLC 1C 2184  
Phenmedipham [77], method, HPLC (revised) J 92  
Phenolphthalein, solution (RE 19) E 267  
d-Phenothrin [777], method L 96  
Phenylurea herbicides, detection and identification of impurities in substituted (MT 142)  F 336 Ob
Phorate [173], method   1B 1890 Ob
Phosalone [109], method   D 141 E
Phosphamidon [110], method, method E 179 E
Phosphate buffer solutions (MT 19)  F 69 Ob
Phosphates, test for (MT 120)  F 285 Ob
Phosphorus in active ingredients, spectrophotometric determination after TLC separation (MT 145)  F 340 Ob
Phosphorus pentoxide desiccant (MT 24)  F 86 Ob
Phoxim [364], method  1C 2187  
Picloram [174], method (salts)  1B 1892 Ob
Picloram [174], method (salts) + 2,4-D [174 + 1] 1B 1757  
Picloram [174], method, HPLC, TC, SL L 104  
Piperonyl butoxide [33], method, TC  1C 2190 Ob
Piperonyl butoxide [33], method, EW
M 163  
Piperonyl butoxide [33], method, LN N 111  
Piperonyl butoxide [33], method + pyrethrum [33 + 32] 1C 2209 Ob
Piperonyl butoxide [33], method + pyrethrum + MGK 264 [33 +32 + 345]
H 239  
Pirimicarb, identity test (MT 164) F 406  
Pirimicarb [231], method H 217  
Pirimiphos-ethyl, identity test (MT 164)  F 406  
Pirimiphos-ethyl [492], method   D 146 Ob
Pirimiphos-methyl, identity test (MT 164)  F 406  
Pirimiphos-methyl [239], method  1C 2192  
Pirimiphos-methyl, pure (PP 239.a)  1C 2337  
Potassium bromate, standard solution (RE 41) E 303  
Potassium bromate/bromide, standard solutions (RE 82)  E 351  
Potassium cyanate [197], method  1C 2200 Ob
Potassium dichromate, standard solutions (RE 20)  E 267  
Potassium dihydrogen orthophosphate (RE 134) E 376  
Potassium hydroxide, standard solutions (RE 21) E 268  
Potassium iodate (RE 98)  E 367  
Potassium iodate/iodide, standard solution (RE 15)  E 264  
Potassium permanganate, standard solution (RE 22) E 270  
Potassium plumbite (RE 75) E 343  
Potassium thiocyanate, standard solution (RE 23)  E 271  
Pour and tap bulk density of granular materials (MT 159) F 390 Ob
Pourability of suspension concentrates (MT 148) F 348  
Pourability of suspension concentrates, revised method (MT 148.1) J 133  
Pour point of mineral oil (MT 139) F 331  
Prallethrin [743] L 110  
Prochloraz [407], method M 165  
Prochloraz [407], EC N 121  
Prochloraz-ZnCl2 Complex, TC N 119  
Procymidon; [383], method K 105  
Profenophos; [461], method H 222  
Prometon [175], method, titration method  1C 2202 Ob
Prometon [175], method, GLC 1C 2203 Ob
Prometryn [93], method H 228  
Propachlor [176], method  D 151  
Propamocarb [399] hydrochloride, method E 184  
Propan-2-ol (RE 40) E 302  
Propazine [92], method H 232 E
Propetamphos [394], method E 187 Ob
Propham + chlorpropham [63 + 43]  1C 2025  
Propiconazole [408], method G 129  
Propineb [177], method   H 236  
Propoxur [80], method  D 155  
Pure pesticides   D 186  
Pyraclostrobin [657], method M 170  
Pyrazophos [350], method  1C 2206 Ob
Pyrethrum [32], method 1C 2209 Ob
Pyrethrum + piperonylbutoxide [32 + 33] 1C 2209 Ob
Pyrethrum + MGK 264 + piperonylbutoxide [32 + 345 + 33] H 239  
Pyridaben [583], method J 94  
Pyridate [447], method G 137  
Pyridine (RE 48) E 310  
Pyriproxyfen [715], method M 178  

Method Book  Page  Status  
Sampling of water dispersible granules (MT 166)  F  415
Sand for germination tests (MT 25) F 86 Ob
Seed adhesion test for powders for seed treatment (MT 83) F 216 Ob
Seed treatment formulations, liquid, determination of seed-seed uniformity of distribution (MT 175) F 438  
Separation and identification of herbicides (MT 97) F 241 Ob
Sethoxydim [401], method E 193  
Sieve analysis, dry sieving-dusts (MT 59.1)
F 177 Ob
Sieve analysis, dry sieving-granular products (MT 59.2) F 179 Ob
Sieve analysis, dry sieving-water dispersible granules (MT 170) F 420  
Sieve analysis, sieve test for granular material (MT 59.4) F 180 Ob
Sieve analysis, wet sieving (MT 59.3) F 179 Ob
Sieve analysis, wet sieving using recycled water (MT 182) J 135  
Sieve analysis, wet sieving-water dispersible granules (MT 167) F 416 Ob
Sieve analysis, wet sieve test (MT 185) K 149  
Silanization of gas chromatographic columns (MT 113) F 277 Ob
Silica for chromatography, silica (MT 21.1) F 71 Ob
Silica for chromatography, sorbisil M 60 (MT 21.2) F 72 Ob
Silica for chromatography, florisil (MT 21.3) F 73 Ob
Silicates, test for (MT 121)  F 287 Ob
Silver diethyldithiocarbamate (RE 44) E 306  
Silver nitrate, standard solutions (RE 24) E

273

 
Simazine [22], method H 250  
Simetryn [179], method, titration method   1B 1895 Ob
Simetryn [179], method, GLC 1B 1896 Ob
Sodium anilinobenzene sulphonate (RE 147) E 383  
Sodium biphenyl (RE 46) E 308  
Sodium bis(2-ethylhexylcarbonyl) ethane sulphonate (RE 71) E 338  
Sodium bis(2-ethylhexyl) sulphosuccinate (RE 71) E 315  
Sodium carbonate (RE 52) E 197  
Sodium chlorate [7], method E 365  
Sodium diethyldithiocarbamate trihydrate (RE 96) E 295  
diSodium dihydrogen ethylenediaminetetra-acetate (RE 37) E 383  
Sodium diphenylaminesulphonate (RE 147) E

273

 
Sodium hydroxide, standard solutions (RE 25) E 299  
Sodium nitrite, standard solutions (RE 39) E 382  
Sodium pentacyanonitrosylferrate(III) (RE 146) E 376  
diSodium tetraborate (RE 133) E 276  
Sodium thiosulphate, standard solutions (RE 26) F 21  
Solubility in acetone (MT 5) F 23  
Solubility in ethanol (MT 7) F 22  
Solubility in hexane (MT 6) H 314  
Solubility in organic solvents (MT 181)

F

200  
Solubility in sodium hydroxide, phenoxyalkanoic herbicides (MT 71.1) F 200  
Solubility in sodium hydroxide, cresols (MT 71.2) F 201  
Solubility in sodium hydroxide, bromoxynil and ioxynil (MT 71.3) F 207 Ob
Solubility in triethanolamine (MT 76) F 262 Ob
Solubility of salts and alkali insoluble-dinitro compounds (MT 108) F 215 Ob
Soluble alkalinity (MT 81) F 215 Ob
Soluble chlorides (MT 82) E 328  
Solvent naphtha, aromatic (RE 62) F 11  
Specific gravity and density, hydrometer method (MT 3.1) F 13  
Specific gravity and density, pyknometer method (MT 3.2) F 18 E
Specific gravity and density, density of suspension concentrates (MT 3.3) L 121  
Spinosad [636], method, TC, SC, GR M 197  
Spontaneity of dispersion, of suspension concentrates (MT 160) F 391  
Spontaneity of dispersion, of water dispersible granules (MT 174) F 435  
Stability of diluted oil products, tar-petroleum oil (MT 55.1) F 167  
Stability of diluted oil products, petroleum and DNOC petroleum oils (MT 55.2)
F 168  
Stability of diluted oil products, petroleum oils for orchard use (MT 55.3)  F 168  
Stability of diluted oil products, petroleum oils for glasshouse use (MT 55.4)  F 168  
Stability of diluted tar and petroleum oil products
F 155  
Stability of diluted tar and petroleum oil products, petroleum oil-miscible type (MT 49.2)
F 156  
Stability of diluted and petroleum oil concentrate products, miscible type (MT 52.1) F 159  
Stability of undiluted DNOC-petroleum, petroleum and tar-petroleum oil products (MT 54) F 167  
Stability of undiluted tar oil products, miscible type (MT 48.1) F 154  
Stability of undiluted tar oil products, stock emulsion type (MT 48.2) F 154  
Stability of tar-petroleum and petroleum oil products-undiluted, miscible type (MT 51.1) F 158  
CIPAC standard waters A - G (MT 18.1) F 59  
CIPAC standard waters H and J (MT 18.2) F 63  
Non CIPAC standard waters (MT 18.3) F 64  
Non CIPAC standard waters, simplified procedure (MT 18.5) H 302  
Starch solution (RE 27) E 280  
Starch indicator paper (RE 32) E 284  
Sulfometuron-methyl [610], method J 108  
Sulfotep [198], method H 255 E
Sulphated ash, general method (MT 29)  F 91  
Sulphur [18], method  K 203  
Sulphuric acid, standard solutions (RE 28) K 280  

Suspensibility of formulations forming suspensions on diluting with water (MT 184)

K 142  
Suspensibility of aqueous suspension concentrates (MT 161) F 394 Ob

Suspensibility of water dispersible granules (MT 168)

F 417 Ob
Suspensibility of water dispersible powders, CIPAC method (MT 15.1) F 45 Ob
Suspensibility of water dispersible powders, AIS method (MT 15.2) F 48  
Suspensibility of water dispersible powders, simplified CIPAC method (MT 177) F 445 Ob
Suspo-emulsions, dispersion stability (MT 180) H 310  

Method Book  Page  Status  
2,4,5-T [6], method, titration method  1C 2220
Ob
2,4,5-T [6], method, GC 1C 2221 Ob
2,4,5-T [6], method, HPLC
1C 2221  
2,4,5-T [6], method - salts 1C 2223  
2,4,5-T [6], method - esters 1C 2223  
2,4,5-T [6], method, 2,4,5-T + 2,4-D [6 + 1]
1C 2072  
2,4,5-T [6], method, 2,4,5-T, pure (PP 6) 1C 2312  
Tannic acid (RE 143) E 376  
Tap density, of powders (MT 33) F 104 Ob
Tap density, of water dispersible granules (MT 169) E 418 Ob/E
2,3,6-TBA [49], method titration method  1C 2225 Ob
2,3,6-TBA [49], method GLC 1C 2227 Ob
2,3,6-TBA [49], method Na-salt, titration method
1C 2228 Ob
2,3,6-TBA [49], method Na-salt, GLC 1C 2229 Ob
2,3,6-TBA + MCPA(salt) [49 + 2] 1C 2148  
2,3,6-TBA, pure (PP49)   1C 2314  
TCDD, determination in 2,4,5-T technical (MT 151.1) F 352  
TCDD, determination in 2,4,5-T technical esters (MT 151.2) E 355  
Tebuconazole [494], method H 261 E
Temephos [340], method  1C 2230  
Terbufos [459], method H 269  
Terbuthylazine [234], method, titration method  1B 1897 Ob
Terbuthylazine [234], method, GLC 1B 1898 Ob
Terbutryn [212], method H 275  
Tetradifon [113], method   1B 1901 Ob
Thallium [181], method   1C 2234 Ob
Thiabendazole [323], method E 211  
Thiacloprid [631], method M 198  
Thiobencarb [388], method  D 159 Ob/E
Thiodicarb [543], method H 279  
Thifensulfuron [452], method K 114  
Thiometon [115], infrared method H 285  
Thiometon [115], gas chromatographic method E 218 Ob
Thiophanate-methyl [362], method D 162  
Thiram [24], method D 169  
Thiram, qualitative procedure for confirmation of the presence of (MT 153) F 360  
Thymol blue, solutions (RE 30) E 283  
Thymolphthalein, solution (RE 30) E 344  
Titanium(III)chloride (RE 83) E 352  
Titanium(III)sulphate (RE 85) E 358  
TMPS, method E 142  
i-TMPS, method E 142  
Toluene (RE 152) E 384  
Toluene solubles (MT 90) F 222 Ob
Tolylfluanid [275], method E 222  
o-Tolyloxyacetic acid (RE 67) E 334  
Total chlorides (MT 100) F 254 Ob
Transfluthrin [741], method K 121  

Transfluthrin [741], method , TC (entantiomeric purity), VL

L 128  
Triadimefon [352], method  1C 2236  
Triadimefon [352], revised method,TC, WP, WG, GR N 126  
Triadimenol [398], method E 224 E
Triadimenol [398], revised method, TC, WP, WG, EC, SC, FS, EW N 134  
Triazophos [353], method H 288  
Tribenuron-methyl [546], method K 128  
1,1,1-Trichloroethane (RE 95) E 365  
Trifluralin [183], method H 292  
Triflumuron [548], method J 114  
Triforine [360], method H 299  
O,O,S-Trimethylphosphorodithioate (RE 87) E 360  
O,O,O-Trimethylphosphorothioate, method E 142  
O,O,S-Trimethylphosphorothioate, method E 142  
(Tris(1,10-phenanthroline)-N,N')iron(II) sulphate (RE 149) E 383  

Method Book  Page  Status  
Xylene (RE 10) E  256
Xylene insoluble material (MT 11) F 30
Xylenol Orange (RE 93) E 364