Pre-published methods

CIPAC Methods are available on a per-method basis, as long as they are not yet published in a Handbook. CIPAC charges a nominal fee per method.

 

Instructions

The list of pre-published methods below is exhaustive.  
Tick the method or methods you wish to receive in the orderform. The methods are sent as pdf files attached to an e-mail - a working e-mail address is therefore mandatory
Each method is charged with GBP 5. Please sum the number of methods you wish to receive and calculate the grand total. Print the form duly filled and signed, to Marston Book Services (see details below) by fax.
As soon as you order is processed, you shall receive the pdf files by e-mail attachment.

 

Terms of Use

By ordering one or more of these methods, the user accepts the conditions of use as follows:

These are draft methods and are subject to revision without further notice
These methods will appear in revised and edited form in CIPAC Handbook O presumably in the year 2016/17. The pre-published methods expire as soon as they appear in printed form in the CIPAC Handbook O.
The CIPAC copyright and disclaimer (cf. CIPAC Handbook L, page ii) applies to all pre-published methods.

 

 

List of available methods

Number
Name
Description
Status
789
Amisulbrom
Reversed phase HPLC method (CIPAC/4883) for the determination of amisulbrom in TC, WG and SC formulations (ISBN 90295184X)
full
570
Chlorfenapyr
Reversed phase HPLC method (CIPAC/4826) for the determination of chlorfenapyr in TC and SC (ISBN 902951912)
full
653
Cyazofamid
Reversed phase HPLC method (CIPAC/4833) for the determination of cyazofamid in TC and SC (ISBN 902951939)
full
333
Deltamethrin
Enantioselective HPLC method (CIPAC/4907) for the determination of the enantiomeric ratio of deltamethrin and its stereoisomers not belonging to the active ingredient definition in TC (ISBN 902951874)
identity test
739
Dimoxystrobin
Capillary GC method (CIPAC/4710) for determination of dimoxystrobin content in TC, SE and SC formulations (ISBN 902951602)
full
595
Flazasulfuron
Reversed phase HPLC method (CIPAC/4831) for the determination of flazasulfuron in TC and WG (ISBN 902951920)
full
521
Fluazinam Reversed phase HPLC method (CIPAC/4727) for the determination of fluazinam in TC and SC formulation (ISBN 902951696)
full
578
Flumioxazin
Reversed phase HPLC method (CIPAC/4763) for the determination of flumioxazin in TC and WP formulations (ISBN 902951629)
full
585
Fosthiazate Reversed phase HPLC method (CIPAC/4829) for the determination of fosthiazate in TC and GR (ISBN 902951793)
full
709
Nicosulfuron
Extension of the scope (CIPAC/4903) of CIPAC method 709/TC/M/3 for the determination of the nicosulfuron content of oil-based suspension concentrate formulations (OD) (ISBN 902951882)
full
331
Permethrin
Method extension to the capillary GC method 331/TC/M/3 (CIPAC/4719,) for the determination of the content of permethrin in EC formulations (ISBN 902951319)
full
33
Piperonyl butoxide
Capillary GC method (CIPAC/4765) for the determination of the content of piperonyl butoxide in TC (ISBN 902951815)
full
239
Pirimiphos-methyl
Capillary GC-FID method (CIPAC/4778) for the determination of total pirimiphos-methyl in TC, EC and CS formulations (ISBN 902951645 ) Revision 2
full
715
Pyriproxyfen
Extension of the scope (CIPAC/4887) of CIPAC method 715/TC/M/2 for the determination of the pyriproxyfen content of a long lasting insecticidal mosquito net (incorporated type) (LN) containing permethrin and pyriproxyfen (ISBN 902951904)
full
636
Spinosad
Method extension to the reversed phase HPLC method 636/TC/M/3 (CIPAC/4721) for the determination of the content of spinosad in EC formulations (ISBN 902951335)
full
636 Spinosad Method extension to the reversed phase HPLC method 636/TC/M/3 (CIPAC/4847) for the determination of the content of spinosad in GR formulations with lower content (ISBN 902951742) full
637
Thiamethoxam
Reversed phase HPLC method (CIPAC/4845) for the determination of thiamethoxam in TC, WG, SC and FS (ISBN 902951785)
full

370

Brodifacoum
The reversed phase HPLC method (CIPAC/4942) for the determination of brodifacoum in TC and RB formulations was accepted as a provisional CIPAC method with the proposal of updating the description of the method concerning standard and sample preparation (ISBN 090295198X)
full
964
Pyraoxystrobin
The reversed phase HPLC method (CIPAC/4936) for the determination of pyraoxystrobin in TC and SC formulations was accepted as a provisional CIPAC method with the proposal of amending the description of the method concerning sonication time and clarification of a possible inclusion of a note concerning addition of water for the sample preparation of the SC (ISBN 978-1-911009-51-1)
full
617
Trifloxystrobin
The reversed phase HPLC method (CIPAC/4954) for the determination of trifloxystrobin in TC, EC, FS, SC, WG and AL formulations was accepted as a provisional CIPAC method with the proposal of amending the description of the method concerning sonication time and clarification of a possible inclusion of a note concerning injection volume (ISBN 978-1-911009-02-3)
full
331 Permethrin The chiral HPLC method (CIPAC/4946) for the determination of the enantiomeric ratio of the four permethrin stereoisomers in technical active substance and EW formulation was accepted as an enantioselective identity test (ISBN 978-1-911009-03-0) adopted
741 Transfluthrin The chiral HPLC method (CIPAC/4948) for the determination of the enantiomeric ratio of the four transfluthrin stereoisomers in technical active substance was accepted as an enantioselective identity test (ISBN 0902951998)
accepted
635 Silthiofam The reversed phase HPLC method using internal standard (CIPAC/5004) for the determination of silthiofam in TC and FS formulations was accepted as a provisional CIPAC method with the inclusion of a note that the addition of the internal standard can be done also volumetrically (ISBN 978-1- 911009-05-4) full
715 Pyriproxyfen The extension of the scope (CIPAC/4997) of CIPAC method 715/TC/M/3 for the determination of the pyriproxyfen content of a matrix release formulation (MR) (incorporated type) was accepted as provisional CIPAC method (ISBN 978-1-911009- 06-1) full
794 Chlorantraniliprole The reversed phase HPLC method using internal standard (CIPAC/5034) for the determination of chlorantraniliprole in TC, FS, WG and SC formulations was accepted as a provisional CIPAC method (ISBN 978-1-911009-09-2).  provisional
693 Fenazaquin The reversed phase HPLC method using external standardisation (CIPAC/5036) for the determination of fenazaquin in TC and SC formulations was accepted as a provisional CIPAC method (ISBN 978-1-911009-10-8).  provisional
454 Alpha-cypermethrin The extension of the scope (CIPAC/5043) of CIPAC method 454/LN/M/3.2 for the determination of the alpha-cypermethrin content of the long lasting insecticidal mosquito net (incorporated type) (LN) containing alpha-cypermethrin and pyriproxyfen, with the modification of having di-cyclohexyl phtalathe as internal standard, instead of dioctyl phtalathe, was accepted as a tentative CIPAC method, with the need for the provision of a second data set according to the provisions of the CIPAC guideline (ISBN 978-1-911009-11-5).
 tentative
738 Clothianidin The extension of the scope (CIPAC/5051) of CIPAC method 738/WG/M/ for the determination of the clothianidin content of WP formulations was accepted as a provisional CIPAC method (ISBN 978-1-911009-13-9).  provisional
       
MT 46.3
Accelerated storage Procedure
The extension of the method MT 46.3 for the accelerated storage procedure of the LN formulations regarding determination of active ingredient content and retention index was accepted as a provisional CIPAC MT method (ISBN 978-1-911009-04-7)
full
NT 47.3 Persistent foam Submethod using a standard measuring cylinder (BS EN ISO 4788:2005) (ISBN 902951831)  full
MT 73.1 Total hardness of water Method for determination of total hardness of water using commercial complexometry (CIPAC/4769) (ISBN 902951718)  full
MT 171.1 Dustiness of granular products

The proposals to make changes in the method for the determination of the dustiness of granular products MT 171 (CIPAC/5003) were accepted with the proposal to include the reason of the revision

This method is free downlodable as a draft version (same condition as a pre-published metod)
 accepted
MT 179.1 Degree of dissolution The extension of the scope (CIPAC/4891) of CIPAC method MT 179 to water soluble formulations (such as SG, SP, SS) was accepted as a provisional CIPAC MT method and the changes proposed to method MT 179.1 were accepted. (ISBN 902951963)  full
MT 189.2 Pirimiphos-methyl Method extension to the CIPAC method MT 189 (CIPAC/4785) for the determination of the content of non-encapsulated pirimiphos-methyl (“free” a.i.) in CS formulations (ISBN 902951653)  full
MT 190.2 Pirimiphos-methyl Method extension to the CIPAC method MT 190 (CIPAC/4783) for the determination of the release rate of pirimiphos-methyl in CS formulations (ISBN 902951661). Revision 2  full
MT 195 Wash resistance index of LN This method is intended for determination of the wash resistance index of long-lasting insecticidal net (LN). It is suitable for coated and incorporated types of LN, in combination with an adopted analytical method for the active ingredient and proper net type (ISBN 902951823)  full
MT 196 Solution properties of ST formulations Method for determination of the residue of soluble tablets retained on a sieve (CIPAC/4771) (ISBN 90295170X)  full
MT 197 Disintegration of tablets Method for the determination of the disintegration of tablets which have to be dissolved or dispersed in water (ST, WT, …) (CIPAC/4894) was accepted as a provisional CIPAC MT method (ISBN 902951971)  full
MT 198 Toluene The headspace GC method (CIPAC/4944) for the determination of toluene in formulations was accepted as a provisional CIPAC MT method (ISBN 0902951947)  full
MT 199 Quaternary ammonium compounds The potentiometric titration method utilizing an ionic surfactant electrode (CIPAC/4965) for the determination of quaternary ammonium compounds in concentrated and ready-to-use (RTU) disinfectant formulations was accepted as a provisional CIPAC method (ISBN 978-1-911009-52-8)  full
MT XXX Retention properties of pyriproxyfen MR formulations The method for the determination of retention properties of pyriproxyfen matrix release formulations (CIPAC/4999) was accepted as a tentative CIPAC MT method with the request of additional validation data (ISBN 978-1-911009-07-8)  tentative
MT 46.3 Accelerated storage Procedure The extension of the scope (CIPAC/5045) of CIPAC method MT 46.3 for the accelerated storage procedure of the MR formulations regarding determination of active ingredient content and retention index was accepted as a tentative CIPAC MT method (ISBN 978-1-911009-12-2).  tentative