MT 105 - Preparation of nitrogen complexes of nitro compounds
Content Handbook F
Outline of method
105.1 Technical compounds
The nitron complex of the compound is prepared and its melting point is determined by a conventional method e.g. MT 2.
The ester is converted to the corresponding phenol with butylamine and hydrochloric acid. The phenol is extracted with petroleum spirit, the solvent is evaporated, and the nitron complex is prepared.