MT 105 - Preparation of nitrogen complexes of nitro compounds

 

Content Handbook F

 

Outline of method

105.1 Technical compounds

The nitron complex of the compound is prepared and its melting point is determined by a conventional method e.g. MT 2.

105.2 Esters

The ester is converted to the corresponding phenol with butylamine and hydrochloric acid. The phenol is extracted with petroleum spirit, the solvent is evaporated, and the nitron complex is prepared.