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Ob: Method "No longer supported"
  E: Errata

Method  Book 
 Page 
 Status 
       
Accelerated storage tests by heating, combined methods (MT 46.1) F  149 Ob
Accelerated storage tests by heating, combined methods (MT 46.2) F 151 Ob
Accelerated storage tests by heating, combined methods (MT 46.3) J 128 Ob
Accelerated storage tests by heating, combined methods (MT 46.3) O 176 Ob
Accelerated storage tests by heating, MR formulations (MT 46.3)  P 230 Ob
Accelerated storage procedure, harmonized method (MT 46.4) P 232  
Acephate [338], method H 5 Ob 
Acephate [338], method, TC, SP P 5  
Acetamiprid [649], method L 4 E
Acetone, anhydrous (RE 34) E 286  
Acetone, soluble material, hot solution (MT 5.1) F 21  
Acetone, solution at room temperature (MT 5.2)      
Acetone, insoluble material (MT 27)      
Acid wash test (MT 79) F 210 Ob
Adhesion to treated seeds (MT 194) N 145  
Acidiy or alkalinity of formulation (MT 191) L 143  
Alachlor [204], method, TC, EC, GR D 4  
Alachlor [204], method, CS E 4 Ob
Aldicarb [215], method H 10 Ob
Aldrin [27], method B 1707 Ob
d-Allethrin [742], method L 16  
d-trans-Allerthrin [203], method H 52  
alpha-Cypermethrin [454], method, TC, WP, EC, SC, UL H 14 E
alpha-Cypermethrin [454], method, SC (oil enhanced), WG K 4  
alpha-Cypermethrin [454], method, LN M 40  
alpha-Cypermethrin [454], and Chlorfenapyr [570], GC method, LN P 62  
alpha-Cypermethrin [454], and Pyriproxyfen [715], GC method, LN P 73  
alpha HCH, in lindane G 106  
Alumina, Brockmann activity grade III (MT 50)  F 156 Ob
Ametryn [133], method, GC H 22 Ob
Ametryn [133], GC method, TC, WG, SC Q 5  
Amisulbrom [789], method, TC, SC, WG O  4  
Amidate, method E 142  
Amines, identification of (MT 152) F 357 Ob
Aminocarb [293] D 9  Ob
2-Aminopyridine, preparation of complexes of nitro compounds (MT 134) F 328 Ob 
Amitraz [362], method G 5 Ob
Amitrole [90], method, potentiometric 1B 1720 Ob
Amitrole [90], method, argentometric 1B 1722 Ob
Amitrole [90], method, HPLC J 4  
Amitrole + monuron [90   + 99] argentometric 1B 1725 Ob
Amitrole + simazin [90   + 22] argentometric, WP 1B 1725 Ob
Amitrole + NH4CNS HPLC J 9  
Amitrole + diuron [90 + 100] HPLC J 9  
Amitrole + terbuthylazine [90 + 234] HPLC J 9  
Ammonia solutions (RE 1) E 245  
Ammonia-ammonium chloride buffer solution-pH 10 (MT 107) F 261  
Ammonium cerium (IV) nitrate (RE 148) E 383  
Ammonium hexanitratocerate (IV) (RE 148) E 383  
d/Ammonium hydrogen citrate (RE 91)      
Ammonium iron (III) sulphate, indicator solution (RE 2) E 246  
d/Ammonium iron (II) sulphate, standard solutions (RE 38)  E 297  
diAmmonium peroxosulphate (RE 132) E 375  
Ammonium thiocyanate, standard solution (RE 3) E 249  
Ammonium trioxovanadate (V), solution (RE 31) E 283  
Anilazine [294], method E 5  
Aromatic solvent naphtha (RE 62) E 328  
Arsenic, determination of (MT 99) F 251  
Arsenic in sulphur, method E 205  
Arsenic in zineb, method E 231  
Arsenic in ziram, method E 237  
Arsenic (III) oxide, standard solution (RE 4) E 250  
Asulam [240], method H 26  
Atrazine [91], method, GC H 37 Ob 
Atrazine [91], method, GC, TC, WG, SC P 12  
Attrition of tablets (MT 193), replaces MT 193 Handbook L, p. 147 O 204 Ob
Attrition resistance of granules (MT 178) H 302 Ob
Attrition resistance of dispersible granules (MT 178.2) K 140 Ob, E
Attrition resistance (MT 178.3), method revision (supersedes MT 178 and MT 178.2) Q 200  
Azadirachtin [627], method M 4  
Azimsulfuron [584], method L 23  
Azinphos-methyl [37], method, HPLC E 12  
Azinphos-methyl [37], method, IR 1C 1970 Ob
Azoxystrobin [571], method M 10 E
Method  Book 
 Page 
 Status 
       
Barium hydroxide, standard solutions (RE 5)  E 251  
Bendiocarb [232], method  D 10  
Benfluralin [285], method, GC  1B 1728 Ob
Benfluralin [285], method, UV  1B 1726 Ob
Benfuracarb [501], method  H 38  
Benomyl [206], method  D 14  
Bensulfuron-methyl [502], method  K 6  
Bensultap [464], method  E 17  
Bentazone [366], method  1C 1973  
Benzoylprop-ethyl [229], method  1B 1732 Ob
Benzoylprop-ethyl, pure (PP 229.a)  1B 1930  
Beta-cyfluthrin [482], method  H 43  
BHC (see HCH)     Ob
BHTO in fenbutatin oxide  D 810  
Bifenox [413], method  G 11  
Binapacryl [138], method  D 67  
Bioallethrin [203], method  H 52 Ob
Bioallethrin [203], TC, LV  L 31  
Bioallethrin + piperonyl butoxide [203 + 33]  H 55 Ob 
S-Bioallethrin [750], method, TC, LV  L 38  
S-Bioallethrin [750], method, EW  M 18  
2,2'-Bipyridyl (RE 61)  E 326  
2,2'-Bipyridyl in diquat  H 161  
4,4'-Bipyridyl (RE 60)  E 325  
4,4'-Bipyridyl in paraquat  H 216 Ob
Bis(ethylenediamine) copper (II) sulphate (RE 81)  E 359  
Bitertanol [386], method  J 14  
Borax (RE 33)  E 376  
Boscalid [673], method  N 4  
Brodifacoum [370], HPLC, method  1C 1981  
Brodifacoum [370], chiral HPLC method, TC, RB  O  12  
Broflanilide [994], HPLC method, TC, WP P 21  
Bromadiolone [371], method      
Bromacil [139], method  1C 1986 Ob
Bromocresol green, solutions (RE 55)  E 317  
Bromophenol blue, solution (RE 6)  E 254  
Bromophos [5], method  1B 1738 Ob
Bromothymol blue, solutions (RE 7)  E 254  
Bromoxynil [87], method  1C 1989  
Bromoxynil pure (PP 87)  1C 2326  
Bromoxynil - octanoate, GC method 1, TC  1C 1998 Ob
Bromoxynil GC method 2, TC,EC 1C 2004 Ob
Bromoxynil pure (PP 87.oct) 1C 2330  
Bromoxynil - heptanoate H 57 Ob
Buffer solutions      
Phosphate buffer (MT 19)  F 69 Ob
Bulk density (MT 186)  K 151  
Bupirimate, identity test (MT 164)  F 406  
Bupirimate [261], method  1C 2007 Ob
Bupirimate, pure (PP 261)  1C 2340  
Butachlor [354], method  D 17 Ob
Butylate [266], method  1B 1744 Ob
Butylmagnesium chloride (RE 139)  E 379  
Method  Book 
 Page 
 Status 
       
Cadmium, standard solution (RE 131) E 374  
Captan [40], method, GC 1C 2015  
Captan [40], method, HPLC 1C 2013  
Carbaryl [26], method M 19  
Carbendazim [263], method, UV H 61  
Carbendazim [263], method, HPLC H 62  
Carbetamide [95], method E 28  
Carbon disulphide (RE 153) E 384  
Carbofuran [276], method D 20  
Carbosulfan [417], method E 35  
Cartap [387], method D 24 Ob/E
Cerium (IV) sulphate, standard solutions (RE 99) E 368  
Cetylpyridinium bromide, solution (RE 11) E 258  
Chinomethionat [172], method 1C 2019 Ob
Chloramben[141], method 1B 1747 Ob
Chlorantraniliprole [794], HPLC method, TC, WG, SC, FS P 28  E
Chlordimeform [277], method D 28 Ob
Chlorfenapyr [570], method, TC, SC O  22  
Chlorfenapyr [570] and alpha-Cypermethrin [454], GC method, LN P 62  
Chlorfenapyr [570] and deltamethrin [333], HPLC method, TC, LN Q 26  
Chlorfenvinphos [88], method H 67 Ob
Chloridazon [111], method D 31  
Chloridazon [111], method extension WG H 76  
Chlorides, in phenoxyalkanoic acids (MT 68.1) F 195 Ob
Chlorides, test for (MT 117) F 282 Ob
Chlorides, total chlorides (MT 100) F 254 Ob
Chlormequat [143], titration method D 39 Ob
Chlormequat, ion chromatographic method H 77  
Chlorobenzilate [119], method H 81 Ob
4-Chloro-m-cresol (RE 104) E 371  
4-Chloro-o-cresol (RE 109)  E 372  
6-Chloro-p-cresol (RE 68)  E 335  
1-Chloro-2,3-epoxyethane (MT 77) F 207 Ob
Chloroform (RE 64) E 330  
Chloroform solubles, hot solutions (MT 87.1) F 221 Ob
Chloroform solubles, cold solutions (MT 87.2) F 222 Ob
6-Chloro-2-methylphenoxyacetic acid (RE 65) E 332  
Gamma-Chlorophosphamidon, method E 182  
Chloropropylate [120], method H 85 Ob
Chlorothalonil [288], method, TC, WP, WG, SC K 13 E
Chlorothalonil + HCB [288 + 161], method, TC, WP, WG, SC K 13 E
6-Chloro-o-tolyloxyacetic acid (RE 65)  E 332  
Chloroxuron [187], method 1B 1751 Ob
Chlorphoxim, [341], method D 24  
Chlorpropham [43], method 1B 1757  
Chlorpropham + propham [43 + 63] 1C 2025  
Chlorpyrifos [221], method, TC, DP, WP, EC, GR 1C 2028  
Chlorpyrifos [221], method extension, UL K 23  
Chlorpyrifos [221], method extension, LN P 47  
Chlorpyrifos [221], HPLC method, TC EC Q 16  
Chlorsulfuron [441], method, TC, WG H 89 E
Chlorsulfuron [441], method extension WP K 24  
Chlorthal [328], method, GC 1C 2032 Ob
Chlorthal [328], method, IR 1C 2034 Ob
Clodinafop [683], method M 26  
Clofentezine [418], method G 18  
Clothianidin [738], method N 14 E
Clothianidin [738], method extension WP P 52  
Conductivity, determination of (MT 32) F 103  
Congo red, solution (RE 9) E 256  
Copper [44], method E 42  
Copper ethylenediamine sulphate (RE 81) E 350  
Copper, water soluble F    
Colorimetric method with bathocuproine (98.1) F 246  
Atomic absorption method (MT 98.2) H 248 Ob
Copper + mancozeb [44 + 34], method H 96  
Copper + maneb [44 + 61], method H 100  
Copper + zineb [44 + 25], method H 100  
Copper + ziram [44 + 31], method F 101  
Correction of interfering peaks (MT 114) F 278 Ob
Coumatetralyl [189], method G 24  
m-Cresol (RE 100) E 370  
o-Cresol (RE 70) E 338  
p-Cresol (RE 101) E 370  
Crystal violet, solution (RE 129)  E 373  
Cyanazine [230], method  1C 2039  
Cyanazine, pure (PP 230) 1C 2335  
Cyazofamid [653], method, TC, SC O 31  E
Cycloate [214], method H 102 Ob
Cyclohexane (RE 155) E 386  
Cycloxydim [510], method K 25  
Cyetpyrafen [997], HPLC method, TC, SC  P  54  
Cyfluthrin [385], method H 106  
beta-Cyfluthrin [482], method H 43  
Lambda-Cyhalothrin [463], method, TC, WP, EC, UL E 49  
Lambda-Cyhalothrin [463], method, LN N 83  
Lambda-Cyhalothrin [463], method, CS K 86  
Lambda-Cyhalothrin, free, determination in CS formulations (MT 189) L 137  
Lambda-Cyhalothrin, determination of release properties CS formulations (MT 190)  L 140 Ob/E
Lambda-Cyhalothrin, determination of release properties of CS formulations (MT 190.1), method revision (replace MT 190) Q 208  
Cyhexatin [289], method D 46  
Cymoxanil [419], method J 22  
Cypermethrin, identity test (MT 163) F 404  
Cypermethrin [332], method, GC 1C 2047 Ob
Cypermethrin [332], method, diastereomeric ratio, HPLC 1C 2052  
Alpha-Cypermethrin [454], method, TC, WP, EC, SC, UL H 14  E
alpha-Cypermethrin [454], method, SC (oil enhanced), WG K 4  
alpha-Cypermethrin [454], method, LN M 40  
alpha-Cypermethrin [454] and Chlorfenapyr [570], GC method, LN P 62  
alpha-Cypermethrin [454] and Pyriproxyfen [715], GC method, LN P 73  
zeta-Cypermethrin [454], HPLC chiral method, TC P 82  
Cyphenothrin [804], method M 44  
Cyphenothrin [804], method extension EW P 93  E
Cyproconazole [600], method J 29  
Cyprodinil [511], method  N 25  
Cyromazin [420], method M 54  
Method  Book            
 Page           
 Status          
       
2,4-D [1], method,  titration method  1C  2060  
2,4-D [1], method,  GC, titration method  1C  2061  
2,4-D [1], method, HPLC, titration method  1C  2062  
2,4-D [1], method,  salts, titration method  1C  2063  
2,4-D [1], method,  salts, titration method, GC  1C  2065  
2,4-D [1], method,  salts, titration method, HPLC  1C  2065  
2,4-D [1], method,  esters, titration method  1C  2068  Ob
2,4-D [1], method,  esters, titration method, GC  1C  2069  
2,4-D [1], method,  esters, titration method, HPLC  1C  2071  
2,4-D + dicamba [1+85] (salts), GC  1C  2071  
2,4-D + dicamba [1+85] (salts), IR  H  133  
2,4-D + dicamba + mecoprop [1 + 85 + 51] (salts)  D  51  
2,4-D + picloram [1 + 174]  1B 1757  Ob
2,4-D + 2,4,5-T [1 + 6] (esters)  1C  2072  
2,4-D, pure (PP 1)  1C  2307  
Dalapon [52], method (Na + Mg salt)  D  54  
Dazomet [146], method, CS2 method  1C  2074  
Dazomet [146], method, CS2 method HPLC   J  37  
2,4-DB [83], method  1C  2078  
2,4-DB [83], K salt,  titration method  1C  2080  
2,4-DB [83], GC  1C  2082  
2,4-DB, pure (PP 83)  1C  2321  
DDT [3], method   E  58  
DDT [3], DDT + endrin [3 + 28]  1B  1760  Ob
Degree of dissolution and solution stability (MT 179.1), replaces MT 179  O 189  
Deltamethrin [333], method, TC, WP, EC, UL, DP  D  57  
Deltamethrin [333], TC, WG, WP, EC, SC, DP, EG, EW, UL, WT (replaced)  L  45  E
Deltamethrin [333], TB, LN  M  65  
Deltamethrin [333], LN  N  34  E
Deltamethrin [333], PE + PP LN incorporated  O 43  
Deltamethrin [333], method, isomers, TC  O 39  
Deltamethrin [333] and chlorfenapyr [570], HPLC method, TC, LN  Q 26  
Desmetryn [147], method, GC  1B  1766  Ob
Desmetryn [147], method, titration method  1B  1765  Ob
Deniges reagent (RE 57)  E  319  
Deschlorophosphamidon, method  E  182  
Detection and identification of impurities in substituted phenylurea herbicides (MT 142)  F  336  Ob
Determination of organochlorine pesticides in aqueous emulsions (MT 65)  F  190  Ob
Determination of pH values, general method (MT 75.1)  F  205  Ob
pH of aqueous dispersions (MT 75.2)  F  206  Ob
pH of diluted and undiluted aqueous solutions (MT 75.3)  J  131  E
Determination of seed-to-seed uniformity of distribution for liquid seed-treament formulations (MT 175)  F  438  
Diazinon [15], method  H  122  Ob
Diazomethane (RE 35)  R  286  
1,2-Dibromoethane [125], method  1C  2115  Ob
Dicamba [85], method, infrared method  H  127  Ob
Dicamba [85], method, HPLC method  K  32  E
Dicamba + 2,4-D [85 + 1], method  H  133  Ob
Dicamba + MCPA [85 + 2], method  H  131  Ob
Dicamba + 2,4-D + mecoprop [85 + 1 + 51] (salts)  D  51  
Dichlobenil [73], method, GC(cap)  E  65  
Dichlobenil [73], GC  1B  1769  Ob
Dichlofluanid [74], method, titration method  1B  1774  Ob
Dichlofluanid [74], method, HPLC  1C  2083  
2,4-Dichlorobenzoic acid (RE 79)  E  347  
Dichlorodifluoromethane insoluble material (MT 16)  F  52  Ob
2,4-dichloroanisole  G  14  
4,6-Dichloro-2-methylphenoxyacetic acid (RE 66)  E  333  
2,4-dichlorophenol  G  14  
4,6-Dichloro-o-tolyloxyacetic acid (RE 66)  E  333  
2,6-Dichlorophenol (RE 72)   E  339  
4,6-Dichloro-o-cresol (RE 69)   E  335  
Dichlorprop [84], method, titration method  1C  2087  
Dichlorprop [84], method, GC  1C  2087  Ob
Dichlorprop [84], method, HPLC  1C  2088  
Dichlorprop [84], HPLC  G  32  
Dichlorprop [84], method, salts, titration method  1C  2092  
Dichlorprop [84], method, salts, GC  1C  2093  
Dichlorprop [84], method, salts, HPLCD initro compounds, solubility of salts and alkali insolubles (MT 108)  1C  2093  Ob
Dichlorprop, pure (PP 84)  1C  2323  
dichlorprop-P [476], method  G  32  
Dichlorvos [11], method, GC  H  135  Ob
Diclofop [358], method  1C  2096  Ob
Dicofol [123], method  D  67  
Dieldrin [16], method  1B  1781  Ob
Diethyl ether (RE 12)  E  258  
Difenoconazole [687], GC method, TC, WG, EC  Q  37  
Diflovidazin [734], method  L  61  
Diflubenzuron [339], method, TC, WP  H  141  
Diflubenzuron [339], method, TC, WP (revised methods)  N  38  
Diflubenzuron [339], method, SC, GR, TB  N  42  
Diflufenican [462], method  H  147  
Dihydrosafrole in piperonyl butoxide, TC  O  104  
Disopropyl ether (RE 63)  E  328  
Dilute emulsion stability (MT 20)  F   71  Ob
Dilute emulsion stability, colorimetric method (MT 173)  F  431  
Dilution stability (MT 41)  F  131  Ob/E
Dilution stability of aqueous solutions (MT 41.1)  O  171  
Dimedone derivative (MT 28)  F  89  Ob
Dimercury dicyanide oxide (RE 154)  E  383  
Dimethoate [59], HPLC method  E  69  
Dimethoate [59], GLC method  H  153  Ob
Dimethomorph [483], method  G  39  
O,O-Dimethyl S-methylcarbamoylmethylphosphorodithioate (RE 86)  E  359  
O,O-Dimethyl methylphosphoroamidothioate, method  E  142  
O,S-Dimethyl methylphosphoroamidothioate, method  E  142  
O,S-Dimethyl 4-nitrophenylphosphorothioate, method  E  169  
O,O-Dimethyl phosphoroamidothioate, method  E  142  
O,O-Dimethyl phosphorochloridothioate, method  O  118  
Dimethyl sulphate (RE 13)  E  259  
Dimoxystrobin [739], method, TC, SE, SC  O  47  
Dinotefuran [749], method  L  67  
Dinotefuran [749], method extension, RB  P  98  
Dinoterb [238], method  1B  1797 Ob
Dinitro compounds, solubility of salts and alkali insolubles (MT 108)  F  262 Ob
Dinitro compounds, solubility of mineral acidity of (MT 109)  F  263 Ob
Dioxane (RE 49)  E  311  
Diquat [55], method  E  74  Ob
Diquat [55], method, identity test  G  47  
Diquat [55], method free 2,2'-bipyridyl  H  161  Ob
Diquat [55], method terpyrides in  M  68  E
Diquat dibromide (PP 55)  E  387  E
Discharge rate of aerosol dispenser (MT 202)  Q  215  
Discharge rate of trigger dispenser (MT 201)  Q  212  
Disintegration of tablets (MT 197)  O  212  
Dispersibility of water dispersible granules (MT 174)  F  435  
Dispersion stability of suspo-emulsions (MT 180)   H  310  
Dispersion stability of suspo-emulsion (MT 180) method extension SE, CD, OD  O  192  
Dissolution rate of water-soluble bags (MT 176)  F  440  
Dissolution degree and solution stability (MT 179)  H  307  
Dissolution degree and solution stability (MT 179.1), replaces MT 179  O  189  E
Disulfoton [152], method  1C  2101  Ob
Dithianon [153], method, HPLC  G  50  
dithianon [153], method, colorimetric  1C  2105  Ob
Dithiocarbamates, determination of anions (MT 154)  F  361  
Identity test for certain alkylenebis (dithiocarbamates) (MT 130)  F  320  
Qualitative procedure for confirmation of the presence of a dithiocarbamate or thiuram disulphide (MT 153)  F  360  
Dithizone (RE 59)  E  371  
Dodine [101], method  1B  1802  Ob/E
Dustability test after accelerated storage (MT 34)  F  107  Ob
Dust content and apparent density of granular formulations, sampling (MT 58.1)  F  173  Ob/E
Dust content and apparent density of granular formulations, preparation of the sample (MT 58.2)  F  173  Ob/E
Dust content and apparent density of granular formulations, apparent density after compactation without pressure (MT 58.3)  F  175  Ob/E
Dustiness of granular products (MT 171)  F  425  Ob/E
Dustiness of granular products (MT 171.1), revised method (supersedes MT 171)  P  235  

 

 

 

Method  Book 
  Page  
  Status  
       
Edifenphos [409], method  E  79  
EDTA sodium salt, solutions (RE 37)  E  295  
Emulsion characteristics of emulsifiable concentrates, five per cent v/v oil phase when diluted (MT 36.1)  F  108 Ob
Emulsion characteristics of emulsifiable concentrates, dispersion stability of aqueous emulsions (MT 36.2)  F  112 Ob
Emulsion characteristics of emulsifiable concentrates, emulsion characteristics and re-emulsification properties (MT 36.3)  K  137  
Emulsion characteristics of emulsifiable concentrates, dilute, colorimetric determination of the stability of emulsions (MT 173)  F  431  
Emulsion characteristics of emulsifiable concentrates, dilute, agrochemical emulsion tester MT 183)  J  138 Ob
Endosulfan [89], method  IC  2111 Ob
Endrin [28], method  1B  1805 Ob
Endrin + DDT [28 + 3]     Ob
Endrin + parathion-methyl [28 + 487]  1B  1819 Ob
Epichlorhydrin (MT 77)  F  207 Ob
Epoxiconazole [609], method  K  38  
EPTC [155], method  1B  1823 Ob
Erichrome Black T (RE 53)  E  316  
Esbiothrin [751], method      
Esfenvalerate [481], method  K  47  
Ethanol soluble material, hot solution (MT 7.1)  F  23  
Ethanol soluble material, solution at room temperature (MT 7.2)  F  24  
Ethephon [373], method  H  165  Ob
Ethephon [373], IC method, TC, TK, SL  Q  46  
Ethiofencarb [363], method  E  84  
Ethion [102], method  1B  1826  
Ethirimol, identity test (MT 164)  F  406  
Ethirimol [242], method  D  72 Ob
Ethofumesate [233], method  J  43  
Ethofumesate [233], SE  L  80  
Ethyl butylacetamidopropionate [667], method  M  76  
N-(2-ethylhexyl)-8,9,10-tribornene-2,3-dicarboxamide [345], method  1C  2166  
Ethylenediamine tetraacetic acid, sodium salt, solutions (RE 37)   E  295  
Etofenprox [471], method (packed column)  G  56  Ob
Etofenprox [471], method (capillary column)  K  57  
ETU, determination in ethylenebisdithiocarbamates (MT 162)  F  399  E
ETU, HPLC method (MT 162.3)  O  180  
Evaluation of wettability, wetting time of a standard type (MT 53.1)  F  160  
Evaluation of wettability, wetting of leaf surfaces (MT 53.2)  F  162  
Evaluation of wettability, wetting of dispersible powders (MT 53.3)  F  164  
Extractable acids, determination of (MT 126)  F  288  
Extractable acids, melting point of (MT 127)  F  291  

 

 
Method  Book 
 Page   Status 
       
Fat extraction apparatus (MT 67) F  194 Ob
Fehling's solution (RE 29) E  262  
Fenazaquin [693], HPLC method, TC, SC P 102  
Fenbutatin oxide [359], method D  77  
Fenhexamid [603], method M  80  
Fenitrothion [35], method N  46  
Fenitrothion [35], method from CIPAC 1C p 2117 was replaced      
Fenobucarb [390], method, TLC D  87 Ob
Fenobucarb [390], method, HPLC D  89 Ob
Fenoprop [118], method, titration method 1C  2121  
Fenoprop [118], method, GC 1C  2122 Ob
Fenoprop [118], method, salts, titration method  1C  2122  
Fenoprop [118], method,GC 1C  2123  
Fenoprop, pure (PP 118) 1C  2333  
Fenoxaprop-P-ethyl [484], method, TC, EW J  51  
Fenoxaprop-P-ethyl [484], method, TC, EW, EC, SE, OD M  89  
Fenpropimorph [427], method G  62  
Fensulfothion [303], method, HPLC 1C  2126 Ob
Fensulfothion [303], method, GC D  92 Ob
Fenthion [79], method, col  1B  1830 Ob
Fenthion [79], method GC, TC, WP, GR, EC, EW L  81  
Fenthion [79], method UL, DP M  96  
Fentin acetate [489], method E  89  
Fentin acetate + maneb [489 + 61], GC 1B  1837 Ob
Fentin acetate + maneb [489 + 61], HPLC E  89  
Fentin hydroxide [490], method E  94  
Fentin hydroxide + maneb [490 + 61] GC 1B  1840 Ob
Fentin hydroxide + maneb [490 + 61] HPLC E  93  
Fenvalerate, identity test (MT 163) F  404  
Fenvalerate [334], method, TC D  101  Ob
Fenvalerate [334], method, EC G  68  Ob
Ferroin sulphate, solution (RE 149) E  383  
Fipronil [581], method TC, EC, UL J  60  
Fipronil [581], method FS, SC, WG, GR, FG N  60  
Flash point, Abel method (MT 12.1) F  31  
Tag closed tester (MT 12.2) F  37  
Pensky-Martens closed tester (MT 12.3) F  40  
Flazasulfuron [595], method, TC, WG O  60  
Florasulamm [616], HPLC method, TC, SC Q  55  
Flowability, of powders (MT 44) F  145  
Flowability, of water dispersible granules (MT 172) F  430  E
Flowability, of granular preparations after accelerated storage under pressure (MT 172.1) O  187  Ob
Flowability, of granular preparations after accelerated storage under pressure, revised method  (MT 172.2), (supersedes MT 172.1) P  241  
Fluazifop-butyl [395], method D  106  
Fluazifop-P-butyl [467], method G  71  
Fluazinam [521], method, TC, SC O  68 E
Flufenoxuron [470], method M  98 E
Flumioxazin [578], method, TC, WP O   77 E
Flumioxazin [578], method extension, suspensibility P  108  
Flumioxazin [578], method extension, SC, WG Q  63  
Fluometuron [159], method 1B 1842 Ob
Flupyradifurone [987], HPLC method, TC, AL, EC, EW, FS, SL, WG P  109  
Flusilazole [435], method H  171  
Folpet [75], method 1B  1845  
Foaming, persistent (MT 47.1) F  152 Ob
Foaming, of suspension concentrates (MT 47.2) F  152 Ob
Foaming, persistent, general method (MT 47.3) O  177 E
Formaldehyde [156], method 1C  2130 Ob
Formothion [160], method H  178 Ob
Fosetyl [384], method, titration method G  82  
Fosetyl [384], method, HPLC J  66  
Fosthiazate [585], metod, TC, GR O  83  
Free acidity or alkalinity, methyl red indicator method (MT 31.1) F  96  
Free acidity or alkalinity, electrometric prodedure (MT 31.2) F  98  
Free acidity or alkalinity, acidity of petroleum products (MT 31.3) F  99  
Free acidity or alkalinity of formulations (MT 191) L  143  
Free acidity of phenoxyalkanoic esters (MT 66) F  193 Ob
Free amines in urea herbicides (MT 141) F  333 Ob
Free 2,2’-bipyridyl in diquat H  161  
Free 4,4’-bipyridyl in paraquat H  216  
Free lambda-cyhalothrin in CS formulations (MT 189) L  137  
Free parathion-methyl in CS formulations (MT 188) L  132  
Free pirimiphos-methyl in CS Formulations (MT 189.2) O  204  
Free phenols in phenoxyalkanoic herbicides, GLC method (MT 69) F  197  
Free phenols in phenoxyalkanoic herbicides, HPLC method (MT 155) F  362  
Freezing mixtures, ( 5 ± 1°C) (MT 14.1) F  44  
Freezing mixtures, (10 ± 1°C) (MT 14.2) F  44  
Freezing point (MT 1) F  3  
Friability of tablets (MT 193) L  147 Ob/E
Friability of tablets (MT 193), replaced by attrition of tablets MT 193 O  204 Ob

 

 

Method  Book  
Page Status 
       
Gas chromatography of phenoxyalkanoic acids and other herbicides (MT 129)  F 292 Ob
Glufosinate [437], method  G 89  
Glyphosate [284], method, TC, SL  1C 2132  
Glyphosate [284], method, SG  H 182  

 

 

 

Method  Book 
 Page 
 Status 
       
Icaridin [740], method K  64 E
Identification of amines (MT 152) F 357 Ob
Identification of urea herbicides (MT 137) F 329 Ob
Identity test for certain dithiocarbamates and thiram and their mixtures (MT 130) F 321  
Identity tests for permethrin, cypermethrin and fenvalerate (MT 163)  F 404  
Identity tests for pirimicarb, bupirimate, ethirimol, pirimiphos-ethyl and pirimiphos-methyl (MT 164)  F 406  
Ignition tests, assessment of spontaneous ignition potential of dithio-carbamates (MT 84.1)  F 218  
Imazalil [335], method E 95 Ob
Imidacloprid [582], method, TC, WP, SC, GR, fertilizer formulations H 185 E
Imidacloprid [582], method, TC, WG, SC, WS, FS K 70  
Imidacloprid [582], method, SL, OD L 89  
Imidacloprid [582], method extension, UL P 133  
Indoxacarb, [612], method, TC, TK, WG, OD, EC N 73 E
Iodides, test for (MT 118) F 283 Ob
Iodine, standard solutions (RE 16) E 264  
Iodine, monochloride, solution (RE 58)  E 320  
Ioxynil [86], method E 101  
Ioxynil octanoate [86.407], method G 94  
Iprobenfos [393], method D 110 Ob
Iprodione [278], method G 98  
Iprodione [278], WG L 90  
IR 3535 see Ethyl butylacetamidopropionate M 76  
Iron, determination of (MT 95)  F 236  
Iron (III) chloride (RE 84) E 355  
Isobutyl benzoate (RE 92) E 362  
Isochloridazone D 35  
Isocycloseram [1025], HPLC method, TC, WP Q 85  
Isofenphos [412], method D 114  
Isolation of active ingredient, extraction with acetone (MT 37.1) F 115 Ob
Isolation of active ingredient, extraction with light petroleum (MT 37.2) F 115 Ob
Isomalathion, method 1B 1855  
Isopirimiphos-methyl in pirimiphos-methyl O 116  
Isoprocarb [396], method D 118 Ob
Isoprothiolane [456], method E 105 Ob
Isoproturon [336], method E 110  
 Method  Book 
 Page   
 Status 
       
John Innes Potting compost for soil testing of seed germination (MT 26) F 87 Ob

 

 

Method  Book 
 Page   Status 
       
Malathion [12], method, TC, DP, WP, EC, OL, (GLC, packed column) 1B 1849 Ob
Malathion [12], method, TC, EC, EW, DP, (GLC, capillary column) K 88  
Mancozeb [34], method H 194  
Mancozeb [34], method + copper [34 + 44] H 96  
Mancozeb [34], HPLC method, TC, WP P 136 E
Manganese, bismuthate method (MT 93.1) F 232  
EDTA method (MT 93.2) E 234  
Magnesium sulphate, solution (RE 144) E 381  
Maneb [61], method E 116 E
Maneb+ copper [61+ 449] H 100  
Maneb+ fentin [61 + 103] E 89  
Maneb+ fentin acetate [61 + 489] D 95  
Maneb+ fentin hydroxide [61 + 490] D 98  
Matrine [1024], HPLC method, TK, SL Q 97  
MCPA [2], titration method 1C 2137 Ob
MCPA [2], GC 1C 2138 Ob
MCPA [2], HPLC 1C 2139  
MCPA [2] - salts,  titration method 1C 2141 Ob
MCPA [2] - salts, GC 1C 2141 Ob
MCPA [2] - salts, HPLC 1C 2141  
MCPA [2] - esters, titration method 1C 2145 Ob
MCPA [2] - esters, GC 1C 2145 Ob
MCPA [2] - esters, HPLC 1C 2145  
MCPA + 2,3,6-TBA [2 + 49] 1C 2148 Ob
MCPA, pure (PP 2) 1C 2309  
MCPB [50], titration method 1C 2153 Ob
MCPB [50], GC 1C 2154 Ob
MCPB [50] - salts, titraton method 1C 2154 Ob
MCPB [50] - salts, GC 1C 2155 Ob
MCPB, pure (PP 50) 1C 2316  
Mecoprop [51], titration method 1C 2157  
Mecoprop [51], GC 1C 2158 Ob
Mecoprop [51], HPLC 1C 2158  
Mecoprop [51] - salts,  titraton method 1C 2162  
Mecoprop [51] - salts,  GC 1C 2163 Ob
Mecoprop [51] - salts,  HPLC 1C 2163  
Mecoprop+ 2,4-D + dicamba [51 + 1 + 8](salts) D 51  
Mecoprop, pure (PP 51) 1C 2319  
Mecoprop-P [475], method  G 109  
Mefenpyr-diethyl, [651.229], method N 87  
Melting point (MT 2) F 5  
Mepiquat [440], method J 78  
Mercurial impurities in technical and formulated mercury compounds (MT 110) F 264  
Mercury, determination on treated seed (MT 158)  F 387 Ob
Mercuric oxycyanide (RE 154) E 385  
Mercury(II)chloride (RE 135) E 378  
Mercury(II) salts, characteristic reactions of (MT 116) F 280 Ob
Mercury(II)sulphate, solution (RE 57) E 319  
Metalaxyl [365], method E 123  
Metamitron [381], method D 124  
Metam-sodium [20], method E 131  
Metazachlor [411], method E 134  
Methabenzthiazuron [201], method  G 116  
Methamidophos [355], method E 139  
Methanol (RE 47) E 309  
Methiocarb [165], method D 130  
Methomyl [264], method H 199 E
Methoprene [414], GC method, TC, EC M 115  
Methoprene [414], method extension, GR, GR-SB, CS Q 104  
Methoprotryne [94], method 1B 1864 Ob
N-Methyl amidate, method E 142  
1-Methylcyclopropene [767], method  N 99  
Methyl (dimethoxyphosphinothioylthio) acetate (RE 88) E 360  
Methyl-methamidophos, method  E 142  
Methyl orange, solutions (RE 17) E 266  
2-Methylphenoxyacetic acid (RE 67) E 334  
Methyl red, solutions (RE 18) E 266  
Methyl undec-10-enoate (RE 89.2) E 361  
Metolachlor [400], method D 134  
Metolachlor [400], GC method, TC, EC, EW Q 110  
Metribuzin [283], method D 137  
Metribuzin [283], GC method, TC, WP, WG, SC Q 119  
Metsulfuron [441], method, TC, WG H 204  
Metsulfuron [441], method extension WP K 95  
Mevinphos [45] H 212  
MGK 264 + pyrethrum + piperonylbutoxide [345 + 32 + 33 ], method H 239  
Mineral acidity of dinitrocompounds (MT 109) F 263 Ob
Mineral oil (RE 36) F   264  
Miscibility with hydrocarbon oil (MT 23) F 85  
Molinate [235], method  1B 1866 Ob
Monocrotophos [287], method E 145  
Mordant black, solutions (RE 53) E 316  
Method  Book  
 Page  
 Status  
       
Packing of columns for gaschromatography (MT 149)  F 349 Ob
Palmitic acid (RE 80)  E 348  
Paraffin, liquid (RE 8) E 255  
Paraquat [56], aqueous solutions, method E 166 Ob
Paraquat [56], aqueous solutions, identity tests G 128  
Paraquat [56], aqueous solutions, free 4,4’-bipyridyl H 216  
Paraquat [56], aqueous solutions, terpyridines in M 141  
Paraquat + diquat [55 + 56], method  E 75 Ob
Paraquat dichloride (PP 55) E 390  
Parathion [10], method, GC  1B 1875 Ob
Parathion [10], method, HPLC 1B 1876 Ob
Parathion-methyl [487], method, GC, TC, WP, EC 1B 1879 Ob
Parathion-methyl [487], method, HPLC, TC, EC 1B 1881 Ob
Parathion-methyl [487], method, HPLC, CS 1C 2169 Ob
Parathion-methyl [487], method, GC, Ol, DP E 171 Ob
Parathion-methyl [487], method, HPLC, OL E 171 OB
Parathion-methyl, free, determination in CS formulations (MT 188)  L 132  
Parathion-methyl, free, HPLC, determination of S-methyl isomer in TC E 169  
Parathion-methyl, free, HPLC, determination of S-methyl isomer in SC E 172  
Particle sizean alysis by laser diffraction (MT 187) K 153 E
Particle size, formulations without carriers (MT 42.1)  F 133 Ob
Particle size, formulations formulations containing carriers (MT 42.2) F 138 Ob
Particle size distribution of a DDT dispersible powder (MT 43)  F 140 Ob
PCAF Reagent (RE 146) E 382  
Pebulate [236], method  1B 1887 Ob
Pencycuron [402], method E 173  
Pendimethanil [357], method M 148  
Pentacyanoaminoferroate (RE 146) E 382  
Perchloric acid, standard solutions (RE 43) E 304  
Permethrin, identity test (MT 163)  F 404  
Permethrin [331], method, TC, WP, EC, WG, DP IC 2173  
Permethrin [331], TC, EW, LN M 155  
Permethrin [331], HPLC, enantiomeric purity in TC, EW O 94  
Permethrin [331], capillary GC + piperonyl butoxide, EC, LN O 97 E
Persistent foaming (MT 47.1)  F 152 Ob
Persistent foam, general method (MT 47.3) O 177 E
Petroleum spirit (RE 45) E 307  
pH, determination of (MT 75)  F 205 Ob
pH, determination of revised method (MT 75.3)  J 131  
Phenmedipham [77], method, titration method 1C 2181  
Phenmedipham [77], method, HPLC 1C 2184  
Phenmedipham [77], method, HPLC (revised) J 92  
Phenolphthalein, solution (RE 19) E 267  
d-Phenothrin [777], method L 96  
Phenylurea herbicides, detection and identification of impurities in substituted (MT 142)  F 336 Ob
Phorate [173], method   1B 1890 Ob
Phosalone [109], method   D 141 E
Phosphamidon [110], method, method E 179 E
Phosphate buffer solutions (MT 19)  F 69 Ob
Phosphates, test for (MT 120)  F 285 Ob
Phosphorus in active ingredients, spectrophotometric determination after TLC separation (MT 145)  F 340 Ob
Phosphorus pentoxide desiccant (MT 24)  F 86 Ob
Phoxim [364], method  1C 2187  
Picloram [174], method (salts)  1B 1893 Ob
Picloram [174], method (salts) + 2,4-D [174 + 1] 1B 1757  
Picloram [174], method, HPLC, TC, SL L 104  
Piperonyl butoxide [33], method, capillary GC, TC O 104 E
Piperonyl butoxide [33], method, TC  1C 2190 Ob
Piperonyl butoxide [33], method, EW M 163  
Piperonyl butoxide [33], method, LN N 111 E
Piperonyl butoxide [33], LN incorporated Q 130  
Piperonyl butoxide [33], LN + deltamethrin O 111  E
Piperonyl butoxide [33], LN + permethrin O 111  E
Piperonyl butoxide [33], method + pyrethrum [33 + 32] 1C 2209 Ob
Piperonyl butoxide [33], method + pyrethrum + MGK 264 [33 +32 + 345] H 239  
Piperonyl butoxide [33], method + dihydrosafrole in, TC O 104  
Piperonyl butoxide [33] and d,d-trans-cyphenothrin [761], method extension, EW P 143  
Pirimicarb, identity test (MT 164) F 406  
Pirimicarb [231], method H 217 Ob
Pirimiphos-ethyl, identity test (MT 164)  F 406  
Pirimiphos-ethyl [492], method   D 146 Ob
Pirimiphos-methyl, identity test (MT 164)  F 406  
Pirimiphos-methyl [239], method  1C 2192  
Pirimiphos-methyl [239], capillary method  GC, EC, CS O 112  
Pirimiphos-methyl [239], capillary method GC, LN Q 134  
Pirimiphos-methyl [239], isopirimiphos-methyl in, TC, CS O 116  
Pirimiphos-methyl [239], O,O-dimethyl phosphorochloridothioate in, TC O 118  
Pirimiphos-methyl [239], O,O,O-trimethyl phosphorothioate in, TC O 118  
Pirimiphos-methyl [239], O,O,S-trimethyl phosphorothioate in, TC O 118  
Pirimiphos-methyl [239], O,O,S-trimethyl phosphorodithioate in, TC O 118  
Pirimiphos-methyl [239], free determination in CS formulations (MT 189.2) O 193  
Pirimiphos-methyl [239], release rate of CS formulations (MT 190.2) O 199  
Pirimiphos-methyl, pure (PP 239.a)  1C 2337  
Potassium bromate, standard solution (RE 41) E 303  
Potassium bromate/bromide, standard solutions (RE 82)  E 351  
Potassium cyanate [197], method  1C 2200 Ob
Potassium dichromate, standard solutions (RE 20)  E 267  
Potassium dihydrogen orthophosphate (RE 134) E 376  
Potassium hydroxide, standard solutions (RE 21) E 268  
Potassium iodate (RE 98)  E 367  
Potassium iodate/iodide, standard solution (RE 15)  E 264  
Potassium permanganate, standard solution (RE 22) E 270  
Potassium plumbite (RE 75) E 343  
Potassium thiocyanate, standard solution (RE 23)  E 271  
Pour and tap bulk density of granular materials (MT 159) F 390 Ob
Pourability of suspension concentrates (MT 148) F 348  
Pourability of suspension concentrates, revised method (MT 148.1) J 133 E
Pour point of mineral oil (MT 139) F 331  
Prallethrin [743], GC method, TC, LV L 110  
Prallethrin [743], method extension, UL P 148  
Prochloraz [407], method M 165  
Prochloraz [407], EC N 121  
Prochloraz-ZnCl2 Complex, TC N 119  
Procymidon; [383], method K 105  
Profenophos; [461], method H 222 Ob
Prometon [175], method, titration method  1C 2202 Ob
Prometon [175], method, GLC 1C 2203 Ob
Prometryn [93], method H 228 Ob
Propachlor [176], method  D 151  
Propamocarb hydrochloride [399], method E 184  
Propan-2-ol (RE 40) E 302  
Propazine [92], method H 232 Ob/E
Propetamphos [394], method E 187 Ob
Propham + chlorpropham [63 + 43]  1C 2025  
Propiconazole [408], method G 129 Ob
Propiconazole [408], GC method, TC, EC P 156  
Propineb [177], method   H 236  
Propoxur [80], method  D 155  
Prothioconazole [745], HPLC method, TC, EC, FS, SC P 164  
Prothioconazole [745], rel. impurity Prothioconazole-desthio, GC-MSMS method, TC, EC, FS, SC Q 140  
Pure pesticides   D 186  
Pyraclostrobin [657], method M 170 E
Pyraoxystrobin [964], method, TC, SC O  134  
Pyrazophos [350], method  1C 2206 Ob
Pyrethrum [32], method 1C 2209 Ob
Pyrethrum + piperonylbutoxide [32 + 33] 1C 2209 Ob
Pyrethrum + MGK 264 + piperonylbutoxide [32 + 345 + 33] H 239 E
Pyridaben [583], method J 94 E
Pyridate [447], method G 137  
Pyridine (RE 48) E 310  
Pyriproxyfen [715], method M 178  
Pyriproxyfen [715], method extension, LN O 143  
Pyriproxyfen [715], method extension, MR P 177  
Pyriproxyfen [715], MR, retention properties method (MT 200) P 255  
Pyriproxyfen [715] and alpha-Cypermethrin [454], HPLC method, LN P 73  

 

 

 

Method  Book  
 Page  
 Status  
       
Sampling of water dispersible granules (MT 166) F 415  
Sand for germination tests (MT 25) F 86 Ob
Seed adhesion test for powders for seed treatment (MT 83) F 216 Ob
Seed treatment formulations, liquid, determination of seed-seed uniformity of distribution (MT 175) F 438  
Separation and identification of herbicides (MT 97) F 241 Ob
Sethoxydim [401], method E 193  
Sieve analysis, dry sieving-dusts (MT 59.1) F 177 Ob
Sieve analysis, dry sieving-granular products (MT 59.2) F 179 Ob
Sieve analysis, dry sieving-water dispersible granules (MT 170) F 420 E
Sieve analysis, sieve test for granular material (MT 59.4) F 180 Ob
Sieve analysis, wet sieving (MT 59.3) F 179 Ob
Sieve analysis, wet sieving using recycled water (MT 182) J 135 Ob
Sieve analysis, wet sieving-water dispersible granules (MT 167) F 416 Ob
Sieve analysis, wet sieve test (MT 185) K 149 Ob
Sieve analysis, wet sieve test (MT 185.1), method revision (supersedes MT 182 and MT 185) Q 205  
Silanization of gas chromatographic columns (MT 113) F 277 Ob
Silica for chromatography, silica (MT 21.1) F 71 Ob
Silica for chromatography, sorbisil M 60 (MT 21.2) F 72 Ob
Silica for chromatography, florisil (MT 21.3) F 73 Ob
Silicates, test for (MT 121)  F 287 Ob
Silthiofam [635], HPLC method, TC, FS P 182  
Silver diethyldithiocarbamate (RE 44) E 306  
Silver nitrate, standard solutions (RE 24)      
Simazine [22], method H 250 Ob
Simetryn [179], method, titration method   1B 1895 Ob
Simetryn [179], method, GLC 1B 1896 Ob
Sodium anilinobenzene sulphonate (RE 147) E 383  
Sodium biphenyl (RE 46) E 308  
Sodium bis(2-ethylhexylcarbonyl) ethane sulphonate (RE 71) E 338  
Sodium bis(2-ethylhexyl) sulphosuccinate (RE 71) E 338  
Sodium carbonate (RE 52) E 315  
Sodium chlorate [7], method E 197  
Sodium diethyldithiocarbamate trihydrate (RE 96) E 365  
diSodium dihydrogen ethylenediaminetetra-acetate (RE 37) E 295  
Sodium diphenylaminesulphonate (RE 147)      
Sodium hydroxide, standard solutions (RE 25) E 273  
Sodium nitrite, standard solutions (RE 39) E 299  
Sodium pentacyanonitrosylferrate(III) (RE 146) E 382  
diSodium tetraborate (RE 133) E 376  
Sodium thiosulphate, standard solutions (RE 26) E 276  
Solubility in acetone (MT 5) F 21  
Solubility in ethanol (MT 7) F 23  
Solubility in hexane (MT 6) F 22  
Solubility in organic solvents (MT 181) H 314  
Solubility in sodium hydroxide, phenoxyalkanoic herbicides (MT 71.1) F 200  
Solubility in sodium hydroxide, cresols (MT 71.2) F 200  
Solubility in sodium hydroxide, bromoxynil and ioxynil (MT 71.3) F 201  
Solubility in triethanolamine (MT 76) F 207 Ob
Solubility of salts and alkali insoluble-dinitro compounds (MT 108) F 262 Ob
Soluble alkalinity (MT 81) F 215 Ob
Soluble chlorides (MT 82) F 215 Ob
Solution properties of water soluble tablets (MT 196) O 210  
Solvent naphtha, aromatic (RE 62) E 328  
Specific gravity and density, hydrometer method (MT 3.1) F 11  
Specific gravity and density, pyknometer method (MT 3.2) F 13  
Specific gravity and density, density of suspension concentrates (MT 3.3) F 18  E
Spinetoram [802], HPLC method, TC, SC, WG, DT Q 158  
Spinosad [636], method, TC, SC, GR L 121  E
Spinosad [636], method extension, DT M 197  
Spinosad [636], method extension, EC, GR O 146  
Spirodiclofen [737], HPLC method, TC, SC P 189  
Spontaneity of dispersion, of suspension concentrates (MT 160) F 391 Ob
Spontaneity of dispersion, of suspension concentrates (MT 160.1), method revision (supersedes MT 160) Q 193  
Stability of diluted oil products, tar-petroleum oil (MT 55.1) F 167  
Stability of diluted oil products, petroleum and DNOC petroleum oils (MT 55.2) F 168  
Stability of diluted oil products, petroleum oils for orchard use (MT 55.3)  F 168  
Stability of diluted oil products, petroleum oils for glasshouse use (MT 55.4)  F 168  
Stability of diluted tar and petroleum oil products, tar-oils-misclibe and stock emulsion types (MT 49.1) F 155  
Stability of diluted tar and petroleum oil products, petroleum oil-miscible type (MT 49.2) F 156  
Stability of diluted and petroleum oil concentrate products, miscible type (MT 52.1) F 159  
Stability of undiluted DNOC-petroleum, petroleum and tar-petroleum oil products (MT 54) F 167  
Stability of undiluted tar oil products, miscible type (MT 48.1) F 154  
Stability of undiluted tar oil products, stock emulsion type (MT 48.2) F 154  
Stability of tar-petroleum and petroleum oil products-undiluted, miscible type (MT 51.1) F 158  
CIPAC standard waters A - G (MT 18.1) F 59  
CIPAC standard waters H and J (MT 18.2) F 63  
Non CIPAC standard waters (MT 18.3) F 64  
Waters of required hardness (MT 18.4) F 66  
Units of measurement for the hardness of water and their conversion (MT 18.5) F 67 E
Standard waters, simplified procedure (MT 18.6) H 302 E
Starch solution (RE 27) E 280  
Starch indicator paper (RE 32) E 284  
Sulfometuron-methyl [610], method J 108  
Sulfotep [198], method H 255 Ob/E
Sulphated ash, general method (MT 29)  F 91  
Sulphur [18], method  E 203  
Sulphuric acid, standard solutions (RE 28) E 280  
Suspensibility of formulations forming suspensions on diluting with water (MT 184) K 142 Ob
Suspensibility of formulations forming suspensions on diluting with water (MT 184.1), (supersedes MT 184) P 245  
Suspensibility of aqueous suspension concentrates (MT 161) F 394 Ob
Suspensibility of water dispersible granules (MT 168) F 417 Ob
Suspensibility of water dispersible powders, CIPAC method (MT 15.1) F 45 Ob
Suspensibility of water dispersible powders, AIS method (MT 15.2) F 48  
Suspensibility of water dispersible powders, simplified CIPAC method (MT 177) F 445 Ob
Suspo-emulsions, dispersion stability (MT 180) H 310  
Suspo-emulsions, dispersion stability (MT 180), method extension SE, CD, OD, method extension SE, CD, OD O 192  

 

 

 

 

 

 

Method  Book         
 Page            Status        
       
2,4,5-T [6], method, titration method  1C 2220 Ob
2,4,5-T [6], method, GC 1C 2221 Ob
2,4,5-T [6], method, HPLC 1C 2221  
2,4,5-T [6], method - salts 1C 2223  
2,4,5-T [6], method - esters 1C 2223  
2,4,5-T [6], method, 2,4,5-T + 2,4-D [6 + 1] 1C 2072  
2,4,5-T [6], method, 2,4,5-T, pure (PP 6) 1C 2312  
Tannic acid (RE 143) E 376  
Tap density, of powders (MT 33) F 104 Ob
Tap density, of water dispersible granules (MT 169) E 418 Ob/E
2,3,6-TBA [49], method titration method  1C 2225 Ob
2,3,6-TBA [49], method GLC 1C 2227 Ob
2,3,6-TBA [49], method Na-salt, titration method 1C 2228 Ob
2,3,6-TBA [49], method Na-salt, GLC 1C 2229 Ob
2,3,6-TBA + MCPA(salt) [49 + 2] 1C 2148  
2,3,6-TBA, pure (PP49)   1C 2314  
TCDD, determination in 2,4,5-T technical (MT 151.1) F 352  
TCDD, determination in 2,4,5-T technical esters (MT 151.2) E 355  
Tebuconazole [494], method H 261 E
Tebuconazole [494], method extension, EC Q 171  
Temephos [340], method  1C 2230  
Terbufos [459], method H 269  
Terbuthylazine [234], method, titration method  1B 1897 Ob
Terbuthylazine [234], method, GLC 1B 1898 Ob
Terbutryn [212], method H 275 Ob
Tetradifon [113], method   1B 1901 Ob
d-Tetramethrin [989], chiral HPLC method, TC P 198  
d-Tetramethrin [989], GC method, TC P 198  
Thallium [181], method   1C 2234 Ob
Thiabendazole [323], method E 211  
Thiacloprid [631], method M 198  
Thiamethoxam [637], method, TC, WG, SC, FS O  147  
Thiobencarb [388], method  D 159 Ob/E
Thiodicarb [543], method H 279  
Thifensulfuron methyl [452], method K 114  
Thiometon [115], infrared method H 285 Ob
Thiometon [115], gas chromatographic method E 218 Ob
Thiophanate-methyl [262], method D 162  
Thiram [24], method D 169  
Thiram, qualitative procedure for confirmation of the presence of (MT 153) F 360  
Thymol blue, solutions (RE 30) E 283  
Thymolphthalein, solution (RE 30) E 344  
Titanium(III)chloride (RE 83) E 352  
Titanium(III)sulphate (RE 85) E 358  
TMPS, method E 142  
i-TMPS, method E 142  
Toluene (RE 152) E 384  
Toluene, method (MT 198) O 215 E
Toluene solubles (MT 90) F 222 Ob
Tolylfluanid [275], method E 222  
o-Tolyloxyacetic acid (RE 67) E 334  
Total chlorides (MT 100) F 254 Ob
Total hardness of water (MT 73.1) O 179  
Transfluthrin [741], GC method, TC, SL K 121  
Transfluthrin [741], GC method , entantiomeric purity, TC, VL L 128 Ob
Transfluthrin [741], HPLC method, identification of isomers, TC O  158 E
Transfluthrin [741], HPLC method, rel. Imp. 1R-trans permethric acid anhydride, TC P 206  
Triadimefon [352], method  1C 2236  
Triadimefon [352], revised method,TC, WP, WG, GR N 126
Triadimenol [398], method E 224 E
Triadimenol [398], revised method, TC, WP, WG, EC, SC, FS, EW N 134  
Triazophos [353], method H 288  
Tribenuron-methyl [546], method K 128  
1,1,1-Trichloroethane (RE 95) E 365  
Trifloxystrobin [617], method, TC, AL, EC, FS, SC, WG O  161 E
Trifloxystrobin [617], HPLC method, relevant impurity CGA 344605, TC, EC, WG, SC Q 173  
Trifluralin [183], method H 292  
Trifluralin [183], HPLC method, TC, EC Q 186  
Triflumuron [548], method J 114  
Triflumuron [548], method, rel. Imp. 1,3-bis(4-trifluoromethoxyphenyl) urea and 4-(trifluoromethoxy) aniline, TC, SC P 212  
Triforine [360], method H 299  
O,O,S-Trimethylphosphorodithioate (RE 87) E 360  
          in pirimiphos-methyl, TC O 118  
O,O,O-Trimethylphosphorothioate, method E 142  
           in pirimiphos-methyl, TC O 118  
O,O,S-Trimethylphosphorothioate, method E 142  
           in pirimiphos-methyl, TC O 118  
(Tris(1,10-phenanthroline)-N,N')iron(II) sulphate (RE 149) E 383  

 

 

 

 

 

 

 

Method  Book  
 Page  
 Status  
       
Xylene (RE 10) E 256  
Xylene insoluble material (MT 11) F 30  
Xylenol Orange (RE 93) E 364  

 

 

 

 

 

 

 

 

Failed to start the session because headers have already been sent by "D:\www\www83\plugins\system\debug\src\Extension\Debug.php" at line 377. (500 Whoops, looks like something went wrong.)

RuntimeException RuntimeException

HTTP 500 Whoops, looks like something went wrong.

Failed to start the session because headers have already been sent by "D:\www\www83\plugins\system\debug\src\Extension\Debug.php" at line 377.

Exceptions 2

RuntimeException

in D:\www\www83\libraries\vendor\joomla\session\src\Storage\NativeStorage.php (line 454)
  1. if ($this->isActive()) {
  2. throw new \RuntimeException('Failed to start the session: already started by PHP.');
  3. }
  5. if (ini_get('session.use_cookies') && headers_sent($file, $line)) {
  6. throw new \RuntimeException(
  7. sprintf('Failed to start the session because headers have already been sent by "%s" at line %d.', $file, $line)
  8. );
  9. }
  11. if (!session_start()) {
NativeStorage->start() in D:\www\www83\libraries\src\Session\Storage\JoomlaStorage.php (line 313)
  1. $this->setId($session_clean);
  2. $cookie->set($session_name, '', ['expires' => time() - 3600 ]);
  3. }
  4. }
  6. parent::start();
  8. // Try loading data from the session
  9. if (!empty($_SESSION['joomla'])) {
  10. $this->data = unserialize(base64_decode($_SESSION['joomla']));
  11. }
JoomlaStorage->start() in D:\www\www83\libraries\vendor\joomla\session\src\Session.php (line 396)
  1. {
  2. if ($this->isStarted()) {
  3. return;
  4. }
  6. $this->store->start();
  8. $this->setState(SessionState::ACTIVE);
  10. // Initialise the session
  11. $this->setCounter();
Session->start() in D:\www\www83\libraries\vendor\joomla\session\src\Session.php (line 327)
  1. * @since 1.0
  2. */
  3. public function has($name)
  4. {
  5. if (!$this->isActive()) {
  6. $this->start();
  7. }
  9. return $this->store->has($name);
  10. }
Session->has() in D:\www\www83\libraries\src\Session\Session.php (line 194)
  2. $name = $args[2] . '.' . $name;
  3. }
  4. }
  6. if (parent::has($name)) {
  7. // Parent is used because of b/c, can be changed in Joomla 6
  8. return parent::get($name, $default);
  9. }
  11. /*
Session->get() in D:\www\www83\libraries\src\Factory.php (line 372)
  1. __CLASS__
  2. ),
  3. E_USER_DEPRECATED
  4. );
  6. $instance = self::getApplication()->getSession()->get('user');
  8. if (\is_null($id)) {
  9. if (!($instance instanceof User)) {
  10. $instance = User::getInstance();
  11. }
Factory::getUser() in D:\www\www83\libraries\src\Document\Renderer\Html\ModulesRenderer.php (line 46)
  1. {
  2. $renderer = $this->_doc->loadRenderer('module');
  3. $buffer = '';
  5. $app = Factory::getApplication();
  6. $user = Factory::getUser();
  7. $frontediting = ($app->isClient('site') && $app->get('frontediting', 1) && !$user->guest);
  8. $menusEditing = ($app->get('frontediting', 1) == 2) && $user->authorise('core.edit', 'com_menus');
  10. foreach (ModuleHelper::getModules($position) as $mod) {
  11. $moduleHtml = $renderer->render($mod, $params, $content);
ModulesRenderer->render() in D:\www\www83\libraries\src\Document\HtmlDocument.php (line 578)
  2. $cbuffer[$hash] = $tmpdata;
  4. $cache->store($cbuffer, 'cbuffer_' . $type);
  5. } else {
  6. $this->setBuffer($renderer->render($name, $attribs, null), $type, $name, $title);
  7. }
  9. return parent::$_buffer[$type][$name][$title];
  10. }
HtmlDocument->getBuffer() in D:\www\www83\libraries\src\Document\HtmlDocument.php (line 897)
  1. $replace = [];
  2. $with = [];
  4. foreach ($this->_template_tags as $jdoc => $args) {
  5. $replace[] = $jdoc;
  6. $with[] = $this->getBuffer($args['type'], $args['name'], $args['attribs']);
  7. }
  9. return str_replace($replace, $with, $this->_template);
  10. }
  11. }
HtmlDocument->_renderTemplate() in D:\www\www83\libraries\src\Document\HtmlDocument.php (line 650)
  2. if (\array_key_exists('csp_nonce', $params) && $params['csp_nonce'] !== null) {
  3. $this->cspNonce = $params['csp_nonce'];
  4. }
  6. $data = $this->_renderTemplate();
  7. parent::render($caching, $params);
  9. return $data;
  10. }
HtmlDocument->render() in D:\www\www83\libraries\src\Document\ErrorDocument.php (line 139)
  1. $this->debug = $params['debug'] ?? false;
  2. $this->error = $this->_error;
  4. $params['file'] = 'error.php';
  6. return parent::render($cache, $params);
  7. }
  9. /**
  10. * Render the backtrace
  11. *
ErrorDocument->render() in D:\www\www83\libraries\src\Error\Renderer\HtmlRenderer.php (line 70)
  1. ob_end_clean();
  2. }
  4. $this->getDocument()->setTitle(Text::_('Error') . ': ' . $error->getCode());
  6. return $this->getDocument()->render(
  7. false,
  8. [
  9. 'template' => $template->template,
  10. 'directory' => JPATH_THEMES,
  11. 'debug' => JDEBUG,
HtmlRenderer->render() in D:\www\www83\libraries\src\Exception\ExceptionHandler.php (line 142)
  1. 'subject' => $app,
  2. 'document' => $renderer->getDocument(),
  3. ])
  4. );
  6. $data = $renderer->render($error);
  8. // If nothing was rendered, just use the message from the Exception
  9. if (empty($data)) {
  10. $data = $error->getMessage();
  11. }
ExceptionHandler::render() in D:\www\www83\libraries\src\Exception\ExceptionHandler.php (line 76)
  1. * @since 3.10.0
  2. */
  3. public static function handleException(\Throwable $error)
  4. {
  5. static::logException($error);
  6. static::render($error);
  7. }
  9. /**
  10. * Render the error page based on an exception.
  11. *
ExceptionHandler::handleException() in D:\www\www83\libraries\src\Application\CMSApplication.php (line 334)
  1. );
  3. // Trigger the onError event.
  4. $this->dispatchEvent('onError', $event);
  6. ExceptionHandler::handleException($event->getError());
  7. }
  9. // Trigger the onBeforeRespond event.
  10. $this->dispatchEvent(
  11. 'onBeforeRespond',
CMSApplication->execute() in D:\www\www83\index.php (line 35)
  2. // Run the application - All executable code should be triggered through this file
  3. require_once dirname(__FILE__) . '/includes/app.php';
  5. $app = JFactory::getApplication('site');
  6. $app->execute();

RuntimeException

Failed to start the session because headers have already been sent by "D:\www\www83\plugins\system\debug\src\Extension\Debug.php" at line 377.

in D:\www\www83\libraries\vendor\joomla\session\src\Storage\NativeStorage.php (line 454)
  1. if ($this->isActive()) {
  2. throw new \RuntimeException('Failed to start the session: already started by PHP.');
  3. }
  5. if (ini_get('session.use_cookies') && headers_sent($file, $line)) {
  6. throw new \RuntimeException(
  7. sprintf('Failed to start the session because headers have already been sent by "%s" at line %d.', $file, $line)
  8. );
  9. }
  11. if (!session_start()) {
NativeStorage->start() in D:\www\www83\libraries\src\Session\Storage\JoomlaStorage.php (line 313)
  1. $this->setId($session_clean);
  2. $cookie->set($session_name, '', ['expires' => time() - 3600 ]);
  3. }
  4. }
  6. parent::start();
  8. // Try loading data from the session
  9. if (!empty($_SESSION['joomla'])) {
  10. $this->data = unserialize(base64_decode($_SESSION['joomla']));
  11. }
JoomlaStorage->start() in D:\www\www83\libraries\vendor\joomla\session\src\Session.php (line 396)
  1. {
  2. if ($this->isStarted()) {
  3. return;
  4. }
  6. $this->store->start();
  8. $this->setState(SessionState::ACTIVE);
  10. // Initialise the session
  11. $this->setCounter();
Session->start() in D:\www\www83\libraries\vendor\joomla\session\src\Session.php (line 327)
  1. * @since 1.0
  2. */
  3. public function has($name)
  4. {
  5. if (!$this->isActive()) {
  6. $this->start();
  7. }
  9. return $this->store->has($name);
  10. }
Session->has() in D:\www\www83\libraries\src\Session\Session.php (line 194)
  2. $name = $args[2] . '.' . $name;
  3. }
  4. }
  6. if (parent::has($name)) {
  7. // Parent is used because of b/c, can be changed in Joomla 6
  8. return parent::get($name, $default);
  9. }
  11. /*
Session->get() in D:\www\www83\libraries\src\Factory.php (line 372)
  1. __CLASS__
  2. ),
  3. E_USER_DEPRECATED
  4. );
  6. $instance = self::getApplication()->getSession()->get('user');
  8. if (\is_null($id)) {
  9. if (!($instance instanceof User)) {
  10. $instance = User::getInstance();
  11. }
Factory::getUser() in D:\www\www83\libraries\src\Application\SiteApplication.php (line 565)
  1. *
  2. * @since 3.2
  3. */
  4. protected function initialiseApp($options = [])
  5. {
  6. $user = Factory::getUser();
  8. // If the user is a guest we populate it with the guest user group.
  9. if ($user->guest) {
  10. $guestUsergroup = ComponentHelper::getParams('com_users')->get('guest_usergroup', 1);
  11. $user->groups = [$guestUsergroup];
SiteApplication->initialiseApp() in D:\www\www83\libraries\src\Application\SiteApplication.php (line 237)
  1. * @since 3.2
  2. */
  3. protected function doExecute()
  4. {
  5. // Initialise the application
  6. $this->initialiseApp();
  8. // Mark afterInitialise in the profiler.
  9. JDEBUG ? $this->profiler->mark('afterInitialise') : null;
  11. // Route the application
SiteApplication->doExecute() in D:\www\www83\libraries\src\Application\CMSApplication.php (line 304)
  1. $this->sanityCheckSystemVariables();
  2. $this->setupLogging();
  3. $this->createExtensionNamespaceMap();
  5. // Perform application routines.
  6. $this->doExecute();
  8. // If we have an application document object, render it.
  9. if ($this->document instanceof \Joomla\CMS\Document\Document) {
  10. // Render the application output.
  11. $this->render();
CMSApplication->execute() in D:\www\www83\index.php (line 35)
  2. // Run the application - All executable code should be triggered through this file
  3. require_once dirname(__FILE__) . '/includes/app.php';
  5. $app = JFactory::getApplication('site');
  6. $app->execute();

Stack Traces 2

[2/2] RuntimeException 
RuntimeException:
Failed to start the session because headers have already been sent by "D:\www\www83\plugins\system\debug\src\Extension\Debug.php" at line 377.

  at D:\www\www83\libraries\vendor\joomla\session\src\Storage\NativeStorage.php:454
  at Joomla\Session\Storage\NativeStorage->start()
     (D:\www\www83\libraries\src\Session\Storage\JoomlaStorage.php:313)
  at Joomla\CMS\Session\Storage\JoomlaStorage->start()
     (D:\www\www83\libraries\vendor\joomla\session\src\Session.php:396)
  at Joomla\Session\Session->start()
     (D:\www\www83\libraries\vendor\joomla\session\src\Session.php:327)
  at Joomla\Session\Session->has()
     (D:\www\www83\libraries\src\Session\Session.php:194)
  at Joomla\CMS\Session\Session->get()
     (D:\www\www83\libraries\src\Factory.php:372)
  at Joomla\CMS\Factory::getUser()
     (D:\www\www83\libraries\src\Document\Renderer\Html\ModulesRenderer.php:46)
  at Joomla\CMS\Document\Renderer\Html\ModulesRenderer->render()
     (D:\www\www83\libraries\src\Document\HtmlDocument.php:578)
  at Joomla\CMS\Document\HtmlDocument->getBuffer()
     (D:\www\www83\libraries\src\Document\HtmlDocument.php:897)
  at Joomla\CMS\Document\HtmlDocument->_renderTemplate()
     (D:\www\www83\libraries\src\Document\HtmlDocument.php:650)
  at Joomla\CMS\Document\HtmlDocument->render()
     (D:\www\www83\libraries\src\Document\ErrorDocument.php:139)
  at Joomla\CMS\Document\ErrorDocument->render()
     (D:\www\www83\libraries\src\Error\Renderer\HtmlRenderer.php:70)
  at Joomla\CMS\Error\Renderer\HtmlRenderer->render()
     (D:\www\www83\libraries\src\Exception\ExceptionHandler.php:142)
  at Joomla\CMS\Exception\ExceptionHandler::render()
     (D:\www\www83\libraries\src\Exception\ExceptionHandler.php:76)
  at Joomla\CMS\Exception\ExceptionHandler::handleException()
     (D:\www\www83\libraries\src\Application\CMSApplication.php:334)
  at Joomla\CMS\Application\CMSApplication->execute()
     (D:\www\www83\index.php:35)
[1/2] RuntimeException 
RuntimeException:
Failed to start the session because headers have already been sent by "D:\www\www83\plugins\system\debug\src\Extension\Debug.php" at line 377.

  at D:\www\www83\libraries\vendor\joomla\session\src\Storage\NativeStorage.php:454
  at Joomla\Session\Storage\NativeStorage->start()
     (D:\www\www83\libraries\src\Session\Storage\JoomlaStorage.php:313)
  at Joomla\CMS\Session\Storage\JoomlaStorage->start()
     (D:\www\www83\libraries\vendor\joomla\session\src\Session.php:396)
  at Joomla\Session\Session->start()
     (D:\www\www83\libraries\vendor\joomla\session\src\Session.php:327)
  at Joomla\Session\Session->has()
     (D:\www\www83\libraries\src\Session\Session.php:194)
  at Joomla\CMS\Session\Session->get()
     (D:\www\www83\libraries\src\Factory.php:372)
  at Joomla\CMS\Factory::getUser()
     (D:\www\www83\libraries\src\Application\SiteApplication.php:565)
  at Joomla\CMS\Application\SiteApplication->initialiseApp()
     (D:\www\www83\libraries\src\Application\SiteApplication.php:237)
  at Joomla\CMS\Application\SiteApplication->doExecute()
     (D:\www\www83\libraries\src\Application\CMSApplication.php:304)
  at Joomla\CMS\Application\CMSApplication->execute()
     (D:\www\www83\index.php:35)